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Acta Cryst. (2012). E68, m1561
[ doi:10.1107/S1600536812048465 ]

trans-Dichloridobis{dicyclohexyl[4-(dimethylamino)phenyl]phosphane-[kappa]P}platinum(II) dichloromethane disolvate

W. L. Davis and R. Meijboom


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT601_ALERT_2_B Structure Contains Solvent Accessible VOIDS of . 127 A   3
Author Response: see _refine_special_details
PLAT922_ALERT_1_B wR2 in the CIF and FCF Differ by ...............    -0.0060      
PLAT927_ALERT_1_B Reported and Calculated  wR2 Differ by .........    -0.0060      
PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers .          1      
PLAT939_ALERT_3_B Large Value of Not (SHELXL) Weight Optimized S .     278.64      

Alert level C PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.593 64 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 2 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1 PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... -0.100
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 10.74 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 91 Perc. PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 5 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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