[Open access]

Acta Cryst. (2012). E68, i91
[ doi:10.1107/S1600536812045667 ]

The layered polyphosphide Ag3.73(4)Zn2.27(4)P16

M. Köpf, O. Osters, M. Bawohl and T. Nilges


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... ? PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms .. ? PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1 Ag7.46 P32 Zn4.54 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.233 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 3 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 3
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 3 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ... ? PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT152_ALERT_1_G The Supplied and Calc. Volume s.1. Differ by ... -5 Units PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag2 -- P2 .. 54.5 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag2 -- P4_e .. 11.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag2 -- P4_g .. 30.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- P1 .. 14.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn1 -- P1 .. 14.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn2 -- P2 .. 54.5 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn2 -- P4_e .. 11.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Zn2 -- P4_g .. 30.0 su PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 22 Perc. PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 16 ALERT level G = General information/check it is not something unexpected 5 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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