[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1463
[ doi:10.1107/S1600536812045655 ]

Bis([mu]-diisopropylhydoxylaminato)-[kappa]2O:N;[kappa]2O:O-bis[(diisopropylhydoxylaminato-[kappa]O)beryllium]

R. J. F. Berger, S. Jana, U. Monkowius and N. W. Mitzel

Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level A
PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low .......      0.919
Author Response: The data were measured using an IPDS-1 with fixed crystal position and therefore completness cannot be achieved. 

Alert level B
PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) .....         27      


Alert level C
REFLT03_ALERT_3_C  Reflection count < 95% complete
           From the CIF: _diffrn_reflns_theta_max           25.77
           From the CIF: _diffrn_reflns_theta_full          25.77
           From the CIF: _reflns_number_total               5220
           TEST2: Reflns within _diffrn_reflns_theta_max
           Count of symmetry unique reflns         5675
           Completeness (_total/calc)             91.98%
RINTA01_ALERT_3_C  The value of Rint is greater than 0.12
            Rint given   0.162
Author Response: No heavy scatteres are present, metal centers are Beryllium. 
PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low ....         45 Perc.
PLAT313_ALERT_2_C Oxygen with three covalent bonds (rare) ........         O3     
PLAT340_ALERT_3_C Low Bond Precision on  C-C Bonds ...............     0.0059 Ang  
PLAT906_ALERT_3_C Large K value in the Analysis of Variance ......      3.536      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600        309      


Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details  in CIF ...          ?
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal ..........    0.02000 Deg. 
PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L=  0.600        123      


   1 ALERT level A = Most likely a serious problem - resolve or explain
   1 ALERT level B = A potentially serious problem, consider carefully
   7 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   3 ALERT level G = General information/check it is not something unexpected

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   8 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster