[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1527
[ doi:10.1107/S1600536812047605 ]

[5-(Pyridin-2-yl)-1H-tetrazole-[kappa]2N4,N5]bis(triphenylphosphane-[kappa]P)copper(I) tetrafluoridoborate

L. Lu, P. Yang, B. Li, L.-F. Shi and H.-R. Cao

Key indicators

checkCIF/PLATON results

No syntax errors found

Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 14
Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.971 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C17 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of B1 PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0078 Ang PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.476 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 103
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.03000 Deg. PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 145
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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