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[Contents scheme]

Acta Cryst. (2012). E68, m1536
[ doi:10.1107/S1600536812045060 ]

Tetrakis(triphenylphosphane-[kappa]P)silver(I) trifluoroacetate ethanol monosolvate

S. W. Ng


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT415_ALERT_2_B Short Inter D-H..H-X H3 .. H11 .. 1.96 Ang.
Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.3 Ratio PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C41 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 50
Alert level G FORMU01_ALERT_1_G There is a discrepancy between the atom counts in the _chemical_formula_sum and _chemical_formula_moiety. This is usually due to the moiety formula being in the wrong format. Atom count from _chemical_formula_sum: C76 H66 Ag1 F3 O3 P4 Atom count from _chemical_formula_moiety:C76 H66 Ag1 F3 O2 P4 PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 26 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 32 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in CIF ... ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- P2 .. 5.8 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- P3 .. 5.5 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ag1 -- P4 .. 5.8 su PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C74 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C73' PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C74' PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C75 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C75' PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 17 Perc. PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 1 PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 218 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 64
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 20 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 8 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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