# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P-1 1.40/0.95 peak/hole Ag1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 174.70 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.7703 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.5987 _cell_length_b 13.7931 _cell_length_c 16.1308 _cell_angle_alpha 89.159 _cell_angle_beta 88.236 _cell_angle_gamma 82.777 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 830.67 763.46 12.59 o 3 0 0 2583.80 2549.68 36.17 o 4 0 0 209.26 216.89 10.90 o 5 0 0 412.85 426.34 16.99 o 6 0 0 250.68 237.51 83.12 o 7 0 0 50.24 28.71 24.55 o 8 0 0 5.51 -3.11 20.83 o 9 0 0 6.46 -13.12 28.22 o -9 1 0 0.31 45.17 57.17 o -8 1 0 54.94 52.60 49.93 o -7 1 0 35.15 15.07 15.73 o -6 1 0 39.89 20.18 13.22 o -5 1 0 274.84 279.42 15.57 o -4 1 0 1627.99 1716.55 23.97 o -3 1 0 1783.49 1723.98 30.93 o -2 1 0 1136.60 1199.72 28.22 o -1 1 0 14155.56 14914.86 184.30 o 2 1 0 22548.98 24639.40 255.38 o 3 1 0 1234.50 1181.20 17.21 o 4 1 0 1254.35 1316.41 36.07 o 5 1 0 1788.24 1905.91 27.81 o 6 1 0 7.45 -0.41 8.54 o 7 1 0 340.46 307.77 92.38 o 8 1 0 0.13 17.81 18.13 o 9 1 0 5.61 29.38 31.61 o -9 2 0 27.62 72.03 41.81 o -8 2 0 328.34 14.83 48.02 o -7 2 0 11.47 5.83 16.54 o -6 2 0 168.07 217.18 20.06 o -5 2 0 138.96 148.93 15.19 o -4 2 0 620.42 603.19 14.73 o -3 2 0 238.92 238.60 9.75 o -2 2 0 1329.56 1288.68 23.71 o -1 2 0 656.42 660.75 43.04 o 1 2 0 5684.58 5543.84 41.65 o 2 2 0 28175.52 32606.35 778.55 o 3 2 0 10.47 12.24 6.92 o 4 2 0 4153.77 4303.54 48.16 o 5 2 0 429.70 438.36 18.87 o 6 2 0 383.36 400.48 24.38 o 7 2 0 3.33 8.41 11.52 o 8 2 0 124.46 34.73 32.06 o 9 2 0 45.67 4.01 50.28 o -9 3 0 24.66 51.99 70.83 o -8 3 0 70.55 3.73 44.44 o -7 3 0 61.09 68.21 34.42 o -6 3 0 759.65 790.69 36.86 o -5 3 0 12.47 18.75 17.16 o -4 3 0 938.16 873.86 28.40 o -3 3 0 2028.19 1869.94 49.75 o -2 3 0 1529.57 1427.09 18.34 o -1 3 0 3095.90 2974.69 64.48 o 0 3 0 465.48 531.22 21.84 o 1 3 0 1632.74 1647.83 20.89 o 2 3 0 12739.09 13133.93 98.32 o 3 3 0 151.08 171.53 4.88 o 4 3 0 2964.86 2845.94 27.87 o 5 3 0 93.88 97.29 11.92 o 6 3 0 105.54 86.40 18.75 o 7 3 0 571.96 599.32 33.43 o 8 3 0 44.64 35.01 13.01 o 9 3 0 30.84 108.84 80.66 o -9 4 0 22.45 -73.57 80.43 o -8 4 0 10.31 0.36 26.46 o -7 4 0 276.19 262.27 48.30 o -6 4 0 765.15 785.86 29.38 o -5 4 0 9.84 -0.23 7.57 o -4 4 0 1956.52 1964.30 81.99 o -3 4 0 854.95 802.20 16.39 o -2 4 0 143.81 135.97 20.46 o -1 4 0 3002.22 2790.31 76.92 o 0 4 0 685.03 750.07 22.33 o 1 4 0 3451.56 3357.77 32.19 o 2 4 0 2893.20 2740.53 28.28 o 3 4 0 2384.52 2538.35 24.39 o 4 4 0 4235.89 4144.73 65.47 o 5 4 0 4.10 7.74 5.98 o 6 4 0 1351.54 1455.90 29.00 o 7 4 0 169.33 147.81 20.27 o 8 4 0 3.18 -4.07 8.73 o 9 4 0 78.22 85.52 51.80 o -9 5 0 5.48 -2.33 36.77 o -8 5 0 37.08 67.63 73.06 o -7 5 0 369.92 306.31 55.26 o -6 5 0 634.94 717.34 61.38 o -5 5 0 278.82 281.15 25.65 o -4 5 0 2282.53 2295.85 74.89 o -3 5 0 1811.53 1847.45 23.71 o -2 5 0 1571.92 1365.22 47.66 o -1 5 0 1437.43 1361.92 24.59 o 0 5 0 1787.47 1724.58 25.98 o 1 5 0 1805.91 1881.68 31.54 o 2 5 0 3024.79 3180.79 57.43 o 3 5 0 1729.06 1677.99 33.99 o 4 5 0 2426.51 2411.89 71.04 o 5 5 0 10.92 30.46 17.75 o 6 5 0 1185.57 1197.66 92.25 o 7 5 0 6.91 -3.74 21.87 o 8 5 0 191.46 210.13 55.90 o 9 5 0 67.49 222.93 104.70 o -8 6 0 0.85 25.90 43.89 o -7 6 0 72.88 100.21 75.17 o -6 6 0 16.35 31.17 35.80 o -5 6 0 1193.53 1331.99 106.10 o -4 6 0 1099.46 1129.42 37.07 o -3 6 0 382.28 375.76 11.97 o -2 6 0 3150.35 3094.59 35.65 o -1 6 0 2753.33 2691.42 38.30 o 0 6 0 2780.20 2801.04 41.99 o 1 6 0 1150.33 1080.70 26.00 o 2 6 0 4.33 10.09 4.66 o 3 6 0 74.25 69.39 6.63 o 4 6 0 129.08 124.23 24.82 o 5 6 0 135.86 158.71 29.76 o 6 6 0 225.37 294.32 32.97 o 7 6 0 35.53 23.95 38.04 o 8 6 0 192.26 368.29 103.39 o 9 6 0 7.02 33.23 51.13 o -8 7 0 11.25 41.29 78.79 o -7 7 0 1.57 76.48 48.51 o -6 7 0 6.17 12.42 34.90 o -5 7 0 260.22 245.87 48.18 o -4 7 0 1092.20 1213.17 65.80 o -3 7 0 197.50 209.68 57.71 o -2 7 0 2249.88 2296.39 43.79 o -1 7 0 110.82 119.44 9.48 o 0 7 0 5089.24 4853.08 68.31 o 1 7 0 3457.58 3444.71 54.02 o 2 7 0 4.32 6.95 5.94 o 3 7 0 132.48 126.57 9.47 o 4 7 0 8.68 9.49 6.56 o 5 7 0 479.16 451.97 40.34 o 6 7 0 214.48 246.76 47.70 o 7 7 0 23.13 -24.05 38.10 o 8 7 0 145.95 272.02 101.51 o 9 7 0 4.46 132.08 104.11 o -7 8 0 106.26 194.84 62.17 o -5 8 0 25.76 21.31 34.09 o -4 8 0 583.57 681.02 59.07 o -3 8 0 799.18 748.63 56.01 o -2 8 0 37.03 41.90 9.51 o -1 8 0 9.76 21.60 11.89 o 0 8 0 3097.93 3002.48 52.10 o 1 8 0 1221.02 1262.31 59.42 o 2 8 0 3630.78 3577.62 44.83 o 3 8 0 2335.91 2364.16 46.57 o 4 8 0 64.91 51.63 8.59 o 5 8 0 523.94 594.95 88.06 o 6 8 0 90.72 58.85 63.14 o 7 8 0 1.99 -42.59 44.24 o 8 8 0 82.44 110.53 58.71 o 9 8 0 0.03 3.87 71.06 o -7 9 0 11.46 121.63 61.10 o -6 9 0 1.30 -10.07 39.85 o -5 9 0 98.92 121.58 78.59 o -4 9 0 0.01 33.71 34.81 o -3 9 0 182.70 215.49 45.87 o -2 9 0 661.62 779.83 44.84 o -1 9 0 768.54 722.70 28.25 o 0 9 0 2417.34 2434.03 101.37 o 1 9 0 52.88 59.98 11.48 o 2 9 0 3784.63 3753.37 53.96 o 3 9 0 735.91 816.89 39.97 o 4 9 0 204.76 204.98 13.02 o 5 9 0 530.23 554.25 90.69 o 6 9 0 89.00 105.48 73.40 o 7 9 0 135.66 157.71 58.53 o 8 9 0 37.21 152.76 63.83 o 9 9 0 24.48 138.54 72.64 o -7 10 0 1.95 -49.07 59.11 o -6 10 0 109.32 142.69 63.19 o -5 10 0 128.70 170.03 92.26 o -4 10 0 84.69 75.67 68.19 o -3 10 0 99.90 24.84 55.16 o -2 10 0 9.45 8.03 11.55 o -1 10 0 1268.12 1327.10 44.78 o 0 10 0 421.57 503.26 24.03 o 1 10 0 1.19 15.96 22.10 o 2 10 0 3088.63 3059.66 53.82 o 3 10 0 0.60 -9.90 9.90 o 4 10 0 1268.23 1223.60 55.05 o 5 10 0 938.65 1080.48 117.13 o 7 10 0 129.37 256.08 65.97 o 8 10 0 12.56 -54.20 58.61 o -6 11 0 155.10 147.85 68.17 o -5 11 0 20.00 76.97 54.50 o -4 11 0 129.11 93.55 51.31 o -3 11 0 6.72 74.15 42.53 o -2 11 0 4.13 -11.72 21.23 o -1 11 0 707.92 765.27 35.88 o 0 11 0 71.23 55.77 41.37 o 1 11 0 757.40 796.60 29.91 o 2 11 0 240.79 267.41 48.66 o 3 11 0 43.04 35.17 13.63 o 4 11 0 1399.32 1301.06 46.75 o 5 11 0 29.88 29.88 7.99 o 6 11 0 154.69 204.17 59.28 o 7 11 0 262.16 348.38 77.66 o 8 11 0 12.53 34.51 58.28 o -6 12 0 61.02 55.09 64.09 o -5 12 0 7.03 34.88 52.15 o -4 12 0 321.90 408.11 75.08 o -3 12 0 143.33 138.54 51.48 o -2 12 0 37.82 36.38 16.09 o -1 12 0 23.95 36.51 23.68 o 0 12 0 79.48 65.57 16.05 o 1 12 0 124.22 146.39 21.25 o 2 12 0 11.55 0.29 12.63 o 3 12 0 111.71 118.51 20.09 o 4 12 0 226.42 193.34 43.95 o 5 12 0 7.44 9.21 9.28 o 6 12 0 317.41 367.70 71.95 o 7 12 0 58.37 113.52 66.01 o 8 12 0 25.70 209.10 83.33 o -2 13 0 450.77 388.90 28.96 o -1 13 0 88.97 84.79 18.94 o 0 13 0 41.10 16.74 18.25 o 1 13 0 91.18 50.90 23.02 o 2 13 0 98.38 60.05 23.99 o 3 13 0 107.50 67.33 33.31 o 4 13 0 72.09 78.68 22.97 o 5 13 0 12.59 9.47 10.16 o 6 13 0 52.90 64.83 54.48 o 7 13 0 12.05 69.39 62.48 o -5 14 0 68.30 42.87 64.62 o -4 14 0 59.56 93.14 66.06 o -3 14 0 0.85 -9.47 43.37 o -2 14 0 339.91 280.94 120.70 o -1 14 0 86.08 59.03 27.51 o 0 14 0 98.10 128.83 23.93 o 1 14 0 590.21 589.24 64.03 o 2 14 0 0.16 -16.74 25.29 o 3 14 0 85.96 52.39 28.06 o 4 14 0 101.27 62.22 20.71 o 5 14 0 4.67 32.42 46.35 o 6 14 0 91.71 64.09 94.77 o 7 14 0 0.13 132.13 116.07 o -4 15 0 8.13 -0.02 27.48 o -3 15 0 17.12 0.32 36.89 o -2 15 0 214.88 196.53 156.61 o -1 15 0 19.02 39.98 28.07 o 0 15 0 277.35 286.62 36.79 o 1 15 0 96.51 70.23 34.65 o 2 15 0 54.82 45.53 23.45 o 3 15 0 48.03 55.82 23.76 o 4 15 0 14.00 26.38 42.46 o 5 15 0 10.06 -27.65 48.49 o 6 15 0 34.55 -64.08 64.08 o -3 16 0 9.70 87.20 68.24 o -2 16 0 42.82 -1.46 40.00 o -1 16 0 0.50 90.99 58.01 o 0 16 0 168.34 136.31 29.24 o 1 16 0 58.75 60.82 25.90 o 2 16 0 15.72 -0.47 16.73 o 3 16 0 62.48 66.29 25.94 o 4 16 0 4.02 -16.41 31.40 o 5 16 0 57.01 74.15 95.85 o -1 17 0 25.52 67.38 57.48 o 0 17 0 161.76 240.44 60.65 o 1 17 0 11.98 27.26 25.22 o 2 17 0 130.46 136.53 33.35 o 3 17 0 37.99 43.88 36.64 o 4 17 0 3.54 27.82 50.26 o -4 -17 1 97.30 72.56 57.76 o -3 -17 1 11.14 68.15 32.63 o -2 -17 1 143.48 162.90 35.26 o -1 -17 1 21.45 53.09 33.89 o 0 -17 1 28.16 11.40 20.00 o 1 -17 1 43.09 133.21 56.64 o -5 -16 1 72.05 63.47 93.61 o -4 -16 1 40.73 61.83 24.00 o -3 -16 1 51.12 76.06 37.32 o -2 -16 1 156.27 96.46 44.97 o -1 -16 1 4.60 41.20 29.93 o 0 -16 1 83.38 111.97 31.67 o 1 -16 1 69.56 145.69 59.60 o 2 -16 1 78.73 -0.73 39.27 o 3 -16 1 2.75 -30.60 58.26 o -6 -15 1 8.62 -33.05 56.08 o -5 -15 1 49.90 78.28 58.27 o -4 -15 1 0.38 23.78 25.41 o -3 -15 1 84.51 89.73 44.20 o -2 -15 1 219.19 132.84 55.13 o -1 -15 1 42.51 37.48 27.57 o 0 -15 1 299.07 288.68 29.57 o 1 -15 1 13.47 13.82 17.42 o 2 -15 1 191.45 139.85 121.68 o 3 -15 1 55.20 1.08 39.52 o 4 -15 1 10.00 0.56 43.11 o -6 -14 1 18.94 72.48 93.91 o -5 -14 1 41.31 71.37 52.69 o -4 -14 1 70.33 86.60 28.39 o -3 -14 1 136.68 110.66 26.39 o -2 -14 1 28.51 14.46 16.47 o -1 -14 1 154.00 163.47 27.72 o 0 -14 1 398.39 418.33 29.77 o 1 -14 1 2.46 7.58 20.22 o 2 -14 1 197.94 158.64 88.26 o 3 -14 1 28.00 -11.89 30.74 o 4 -14 1 118.44 27.84 38.76 o 5 -14 1 70.09 95.03 73.11 o -7 -13 1 5.67 69.90 62.36 o -6 -13 1 33.35 51.75 54.23 o -5 -13 1 28.45 25.49 11.48 o -4 -13 1 59.70 75.84 24.33 o -3 -13 1 78.21 61.59 19.28 o -2 -13 1 55.62 66.59 20.72 o -1 -13 1 319.70 330.80 28.00 o 0 -13 1 24.21 32.79 18.47 o 1 -13 1 174.71 184.93 27.10 o 2 -13 1 95.19 61.19 30.42 o 3 -13 1 88.88 -3.01 36.21 o 4 -13 1 190.90 -0.40 36.28 o 5 -13 1 17.55 45.16 57.68 o -8 -12 1 23.39 115.37 72.89 o -7 -12 1 6.02 12.31 48.05 o -6 -12 1 199.55 318.55 70.55 o -5 -12 1 43.40 32.43 22.01 o -4 -12 1 134.51 64.78 32.13 o -3 -12 1 56.60 52.80 16.76 o -2 -12 1 375.95 348.03 28.75 o -1 -12 1 101.08 77.01 17.40 o 0 -12 1 595.21 634.34 36.43 o 1 -12 1 753.83 759.73 33.52 o 2 -12 1 359.90 354.69 61.60 o 3 -12 1 127.16 76.65 59.57 o 4 -12 1 62.64 105.21 54.90 o 5 -12 1 8.07 39.31 53.41 o 6 -12 1 30.76 24.94 55.65 o -8 -11 1 40.20 128.02 71.36 o -7 -11 1 56.73 56.27 52.64 o -6 -11 1 65.78 181.02 58.44 o -5 -11 1 9.64 4.09 10.19 o -4 -11 1 532.43 527.06 28.17 o -3 -11 1 18.72 12.92 15.47 o -2 -11 1 41.89 33.67 15.35 o -1 -11 1 1694.27 1722.14 45.36 o 0 -11 1 83.80 91.34 19.36 o 1 -11 1 238.34 231.50 69.07 o 2 -11 1 727.78 739.00 123.47 o 3 -11 1 12.71 14.80 36.25 o 4 -11 1 94.63 112.75 77.76 o 5 -11 1 59.97 79.46 53.77 o 6 -11 1 22.17 -5.57 44.77 o -8 -10 1 72.37 64.37 58.95 o -7 -10 1 53.07 -16.67 43.72 o -5 -10 1 268.00 208.26 21.86 o -4 -10 1 1243.67 1226.62 45.80 o -3 -10 1 41.36 31.34 12.31 o -2 -10 1 832.39 836.04 27.48 o -1 -10 1 691.35 717.33 35.27 o 0 -10 1 449.74 505.82 32.66 o 1 -10 1 176.46 178.03 23.38 o 2 -10 1 234.62 262.63 46.34 o 3 -10 1 241.71 222.09 13.77 o 4 -10 1 167.08 166.02 52.72 o 6 -10 1 274.60 334.89 73.53 o 7 -10 1 0.45 8.62 48.24 o -8 -9 1 14.10 -5.39 41.92 o -7 -9 1 159.49 259.52 62.86 o -6 -9 1 141.70 111.39 75.18 o -5 -9 1 373.41 342.05 26.56 o -4 -9 1 354.72 367.27 29.11 o -3 -9 1 65.48 70.72 12.15 o -2 -9 1 4447.85 4524.53 62.99 o -1 -9 1 453.31 477.01 23.86 o 0 -9 1 954.95 976.07 31.17 o 1 -9 1 1011.95 999.69 37.95 o 2 -9 1 5.19 24.74 13.89 o 3 -9 1 424.82 400.64 29.32 o 4 -9 1 36.91 -2.58 29.00 o 5 -9 1 75.52 95.75 45.31 o 6 -9 1 5.46 63.55 78.40 o 7 -9 1 6.72 31.49 50.94 o -8 -8 1 94.04 124.64 59.25 o -7 -8 1 101.30 39.03 43.21 o -6 -8 1 0.47 -10.75 50.97 o -5 -8 1 580.48 620.07 109.14 o -4 -8 1 494.74 495.21 39.13 o -3 -8 1 841.93 838.39 33.18 o -2 -8 1 8917.87 8455.39 86.73 o -1 -8 1 4.18 0.43 8.20 o 0 -8 1 2674.31 2464.43 55.96 o 1 -8 1 396.12 379.58 16.82 o 2 -8 1 145.94 169.31 29.88 o 3 -8 1 713.70 764.72 56.98 o 4 -8 1 49.57 55.35 37.30 o 5 -8 1 37.55 69.66 40.10 o 7 -8 1 23.27 80.38 53.26 o -9 -7 1 0.28 0.43 37.08 o -8 -7 1 83.70 140.18 56.29 o -7 -7 1 11.84 -12.44 35.57 o -6 -7 1 206.48 216.06 74.76 o -5 -7 1 483.07 447.20 24.02 o -4 -7 1 39.01 36.88 18.09 o -3 -7 1 616.56 526.41 22.18 o -2 -7 1 6411.55 6294.84 84.78 o -1 -7 1 96.16 96.99 28.99 o 0 -7 1 3238.17 2969.17 44.16 o 1 -7 1 1254.28 1254.94 48.25 o 2 -7 1 2916.41 3040.31 113.67 o 3 -7 1 982.91 969.66 55.70 o 4 -7 1 337.69 328.23 13.29 o 5 -7 1 435.54 426.72 21.40 o 6 -7 1 198.29 79.78 70.92 o 7 -7 1 7.17 109.20 51.77 o 8 -7 1 1.39 36.87 77.74 o -9 -6 1 1.88 18.84 46.57 o -8 -6 1 131.25 203.06 91.50 o -7 -6 1 146.13 117.11 45.38 o -6 -6 1 17.39 -22.73 49.86 o -5 -6 1 560.83 507.25 22.19 o -4 -6 1 300.09 365.27 33.36 o -3 -6 1 1468.12 1334.07 32.16 o -2 -6 1 590.55 542.58 22.54 o -1 -6 1 273.84 259.54 17.34 o 0 -6 1 3589.10 3319.78 44.47 o 1 -6 1 809.51 814.66 54.72 o 2 -6 1 5289.20 5183.96 111.99 o 3 -6 1 540.66 520.24 23.35 o 4 -6 1 581.72 593.52 58.41 o 5 -6 1 810.84 814.09 28.45 o 6 -6 1 12.45 -4.48 13.90 o 7 -6 1 135.08 164.45 51.81 o 8 -6 1 60.61 152.20 55.85 o -9 -5 1 69.22 57.17 80.62 o -8 -5 1 311.44 370.07 63.59 o -7 -5 1 11.15 1.42 8.92 o -6 -5 1 592.97 622.73 47.06 o -5 -5 1 167.94 142.13 23.81 o -4 -5 1 49.44 48.56 6.43 o -3 -5 1 1216.53 1133.59 17.22 o -2 -5 1 163.80 136.67 9.57 o -1 -5 1 4.66 17.09 14.12 o 1 -5 1 792.96 734.87 31.95 o 2 -5 1 7126.68 6452.17 124.71 o 3 -5 1 0.70 8.24 7.63 o 4 -5 1 936.19 995.82 35.62 o 5 -5 1 384.82 313.38 22.35 o 6 -5 1 375.68 414.57 29.40 o 7 -5 1 177.19 162.63 20.86 o 8 -5 1 2.87 38.13 41.43 o 9 -5 1 15.06 54.43 35.36 o -9 -4 1 198.20 261.58 65.28 o -8 -4 1 113.09 103.79 70.08 o -7 -4 1 25.73 27.10 16.35 o -6 -4 1 1852.32 1891.28 45.29 o -5 -4 1 239.00 232.16 12.09 o -4 -4 1 14.41 25.16 11.53 o -3 -4 1 5713.18 5733.23 48.29 o -2 -4 1 4248.54 4280.71 40.25 o -1 -4 1 826.05 752.77 16.68 o 1 -4 1 2445.71 2311.68 52.76 o 2 -4 1 2064.05 1921.67 70.85 o 3 -4 1 242.80 223.56 9.96 o 4 -4 1 2047.02 2166.34 50.31 o 5 -4 1 287.90 266.36 51.32 o 6 -4 1 276.93 314.68 25.93 o 7 -4 1 180.26 176.69 43.89 o 8 -4 1 0.00 11.73 53.11 o 9 -4 1 34.68 128.79 45.74 o -9 -3 1 105.13 160.57 85.68 o -8 -3 1 173.27 84.61 48.93 o -7 -3 1 428.82 422.60 25.45 o -6 -3 1 517.95 536.23 17.82 o -5 -3 1 424.03 442.67 15.04 o -4 -3 1 2017.61 1969.65 40.68 o -3 -3 1 61.41 61.15 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