[Open access]

[Contents scheme]

Acta Cryst. (2012). E68, m1508-m1509
[ doi:10.1107/S1600536812046971 ]

trans-Dichloridobis{tris[4-(trifluoromethyl)phenyl]phosphane-[kappa]P}palladium(II) dichloromethane monosolvate

W. L. Davis and A. Muller


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT213_ALERT_2_C Atom F15 has ADP max/min Ratio ..... 3.2 prola PLAT215_ALERT_3_C Disordered F10A has ADP max/min Ratio ..... 3.1 PLAT215_ALERT_3_C Disordered F11B has ADP max/min Ratio ..... 3.2 PLAT215_ALERT_3_C Disordered F12A has ADP max/min Ratio ..... 3.1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C4
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 16 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Pd2 -- P2 .. 7.0 su PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 11 Perc. PLAT434_ALERT_2_G Short Inter HL..HL Contact F3 .. F15 . 2.77 Ang. PLAT434_ALERT_2_G Short Inter HL..HL Contact F8 .. F12A . 2.78 Ang. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 116 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 25
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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