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[Contents scheme]

Acta Cryst. (2012). E68, m1565-m1566
[ doi:10.1107/S1600536812048222 ]

Di-[mu]-chlorido-bis({8-[bis(naphthalen-1-yl)phosphanyl]naphthalen-1-yl-[kappa]2C1,P}palladium(II)) dichloromethane disolvate

W. L. Davis and A. Muller


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT213_ALERT_2_C Atom C6 has ADP max/min Ratio ..... 3.1 prola PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C31 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.2 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 39 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 5 PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density 1.60 eA-3 PLAT971_ALERT_2_C Large Calcd. Non-Metal Positive Residual Density 1.56 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -2.37 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -2.26 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -2.09 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -2.09 eA-3 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -1.83 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 7.03 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 49
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 10 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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