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Acta Cryst. (2013). E69, m29-m30
[ doi:10.1107/S1600536812047964 ]

catena-Poly[[[O,O'-bis(2-methylphenyl) dithiophosphato-[kappa]2S,S]lead(II)]-[mu]-O,O'-bis(2-methylphenyl) dithiophosphato-[kappa]3S,S':S]

R. J. Butcher, R. Ratnani, S. Öztürk Yildirim and O. Falola


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT915_ALERT_3_B Low Friedel Pair Coverage ...................... 38 Perc.
Alert level C PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0123 Ang
Alert level G REFLT03_ALERT_4_G WARNING: Large fraction of Friedel related reflns may be needed to determine absolute structure From the CIF: _diffrn_reflns_theta_max 75.59 From the CIF: _reflns_number_total 4494 Count of symmetry unique reflns 3401 Completeness (_total/calc) 132.14% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 1093 Fraction of Friedel pairs measured 0.321 Are heavy atom types Z>Si present yes PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 16 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 9 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 21 Perc. PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF .... # 9 O4 -P2 -O4A 1.555 1.555 1.555 21.90 Deg. PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 55 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 52
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 1 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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