Acta Cryst. (2013). E69, m4
[ doi:10.1107/S160053681204888X ]

Hexa-₂-acetato-hexa-n-butylhexa-₃-oxido-tin(IV) toluene monosolvate

M. Reichelt and H. Reuter

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.005 Å
• Disorder in main residue
• R factor = 0.020
• wR factor = 0.046
• Data-to-parameter ratio = 20.9

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......      0.958      
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...        4.7 Ratio

Alert level C
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C42     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors of         C43     
PLAT331_ALERT_2_C Small Average Phenyl   C-C Dist. C42    -C43_b         1.36 Ang. 
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .         56 A   3 
PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) .....          4      
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600         77      
PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF ....          1      

Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          8      
PLAT005_ALERT_5_G No _iucr_refine_instructions_details  in the CIF          ?
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large.       9.92      
PLAT301_ALERT_3_G Note: Main Residue  Disorder ...................         13 Perc.
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          6      
PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L=  0.600        214      

   0 ALERT level A = Most likely a serious problem - resolve or explain
   2 ALERT level B = A potentially serious problem, consider carefully
   7 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   6 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   6 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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