[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m4
[ doi:10.1107/S160053681204888X ]

Hexa-[mu]2-acetato-hexa-n-butylhexa-[mu]3-oxido-tin(IV) toluene monosolvate

M. Reichelt and H. Reuter


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low ....... 0.958 PLAT220_ALERT_2_B Large Non-Solvent C Ueq(max)/Ueq(min) ... 4.7 Ratio
Alert level C PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C42 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C43 PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C42 -C43_b 1.36 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 56 A   3 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 77 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 8 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 9.92 PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 13 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 6 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 214
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster