Acta Cryst. (2013). E69, m3
[ doi:10.1107/S1600536812046958 ]

Bis({1-[(1-iminoethyl)imino]ethyl}azanido-²N¹,N⁵)nickel(II) methanol monosolvate

Y.-Q. Xie, J.-J. Li, Y. Guo, Y.-M. Zhang and T.-B. Wei

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.004 Å
• R factor = 0.029
• wR factor = 0.082
• Data-to-parameter ratio = 14.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ...     -5.000      

Alert level G
PLAT005_ALERT_5_G No _iucr_refine_instructions_details  in the CIF          ?
PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............          5      
PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels ..........          4      
PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still          42 Perc.

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   1 ALERT level C = Check. Ensure it is not caused by an omission or oversight
   4 ALERT level G = General information/check it is not something unexpected

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   2 ALERT type 5 Informative message, check

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