# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' hc187 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 399.35 _exptl_crystal_F_000 1402.00 _reflns_d_resolution_high 0.7997 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.0315 _cell_length_b 13.3638 _cell_length_c 19.3489 _cell_angle_alpha 96.358 _cell_angle_beta 99.229 _cell_angle_gamma 116.191 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 70.42 199.01 15.15 o 3 0 0 29253.32 29876.54 442.14 o 4 0 0 61295.18 58219.74 836.78 o 5 0 0 23146.29 23636.29 331.60 o 6 0 0 1390.63 1341.58 31.20 o 7 0 0 4515.11 4308.89 83.85 o 8 0 0 9855.63 9329.78 160.42 o 9 0 0 6970.80 7365.46 156.00 o 10 0 0 102.98 207.96 37.70 o 11 0 0 22.76 43.19 43.10 o 12 0 0 3872.22 3654.05 212.93 o 13 0 0 2112.13 1908.15 151.52 o 14 0 0 52.75 -113.32 119.01 o -14 1 0 2078.24 2567.18 275.37 o -13 1 0 14.82 13.24 94.74 o -12 1 0 593.88 793.69 69.81 o -11 1 0 7318.15 8114.21 240.76 o -10 1 0 6232.08 6862.35 159.62 o -9 1 0 760.23 859.28 32.81 o -8 1 0 188.16 200.17 19.22 o -7 1 0 10626.39 9960.85 178.81 o -6 1 0 14904.58 15176.13 230.11 o -5 1 0 363.61 424.56 21.34 o -4 1 0 21381.54 21225.00 292.16 o -3 1 0 31309.94 30589.47 454.05 o -2 1 0 10210.83 9866.96 158.99 o -1 1 0 390.28 -4.90 4.90 o 1 1 0 10759.10 11876.90 159.51 o 2 1 0 41023.96 41246.25 509.78 o 3 1 0 1142.58 825.21 19.96 o 4 1 0 28984.31 27462.80 338.50 o 5 1 0 6491.62 6766.00 100.50 o 6 1 0 308.50 398.49 21.99 o 7 1 0 4078.17 4100.48 78.15 o 8 1 0 16995.77 17146.54 331.64 o 9 1 0 5356.57 5573.69 129.67 o 10 1 0 540.17 679.61 41.33 o 11 1 0 771.41 984.87 58.09 o 12 1 0 5593.75 6070.74 375.98 o 13 1 0 3601.24 3971.59 396.76 o -15 2 0 1483.87 1373.48 190.01 o -14 2 0 1240.66 994.84 167.34 o -13 2 0 8.54 5.47 63.88 o -12 2 0 211.70 117.64 50.93 o -11 2 0 6803.65 6743.40 179.31 o -10 2 0 10834.56 11080.42 255.81 o -9 2 0 1614.97 1532.26 44.33 o -8 2 0 3536.15 3803.97 92.49 o -7 2 0 43565.77 42303.95 658.28 o -6 2 0 49587.08 48749.61 683.35 o -5 2 0 5598.48 5873.19 91.76 o -4 2 0 2153.13 2133.73 40.96 o -3 2 0 59819.44 60533.37 840.83 o -2 2 0 111231.70 106639.58 1754.41 o -1 2 0 4009.06 4331.89 85.86 o 0 2 0 756.72 1080.90 19.48 o 1 2 0 152610.23 151378.86 2238.15 o 2 2 0 86708.33 85208.48 1087.10 o 3 2 0 51430.83 52506.26 667.27 o 4 2 0 1983.39 2656.86 42.10 o 5 2 0 7234.09 6821.36 96.32 o 6 2 0 11374.48 10964.53 178.79 o 7 2 0 2126.26 2339.78 59.14 o 8 2 0 350.74 400.22 27.88 o 9 2 0 3.27 -4.54 27.42 o 10 2 0 3026.95 2655.63 94.32 o 11 2 0 598.78 603.70 63.42 o 12 2 0 1125.74 1385.06 199.14 o 13 2 0 295.41 321.34 115.45 o -15 3 0 24.83 -206.62 206.62 o -14 3 0 577.76 672.58 92.03 o -13 3 0 6950.33 7447.21 329.02 o -12 3 0 2237.68 2263.62 90.51 o -11 3 0 610.93 547.29 42.20 o -10 3 0 98.59 216.88 43.54 o -9 3 0 9902.81 10222.35 223.71 o -8 3 0 4554.84 4467.89 94.12 o -7 3 0 3409.81 2809.56 55.74 o -6 3 0 825.85 795.16 25.67 o -5 3 0 24565.43 23095.48 350.54 o -4 3 0 2404.52 2550.95 45.75 o -3 3 0 54630.77 53903.28 938.95 o -2 3 0 17899.08 18617.66 380.46 o -1 3 0 11.53 67.43 13.37 o 0 3 0 21161.66 20743.45 394.27 o 1 3 0 49001.20 47021.29 732.49 o 2 3 0 29162.13 28876.69 412.31 o 3 3 0 16680.72 17096.05 235.84 o 4 3 0 17.13 36.38 18.97 o 5 3 0 5038.71 4744.61 84.24 o 6 3 0 15086.07 15255.93 256.10 o 7 3 0 2822.22 2994.28 70.36 o 8 3 0 262.08 323.46 37.86 o 9 3 0 4317.94 4520.32 128.90 o 10 3 0 7487.52 7715.81 252.73 o 11 3 0 1979.13 2133.99 175.10 o 12 3 0 94.25 71.31 123.14 o -15 4 0 3.54 -27.20 187.91 o -14 4 0 2425.48 2390.61 177.82 o -13 4 0 10371.64 10813.84 387.67 o -12 4 0 1644.73 1769.67 85.54 o -11 4 0 20.50 -41.66 41.66 o -10 4 0 7921.28 7394.25 189.01 o -9 4 0 27738.32 28967.65 516.55 o -8 4 0 17277.52 17054.74 317.60 o -7 4 0 100.88 115.59 19.12 o -6 4 0 14939.56 15057.96 229.55 o -5 4 0 93535.40 93304.42 1367.83 o -4 4 0 46787.54 45516.19 789.38 o -3 4 0 2768.66 2749.76 59.73 o -2 4 0 20618.23 21215.62 437.65 o -1 4 0 24665.09 24725.11 408.70 o 0 4 0 30759.99 30286.53 542.83 o 1 4 0 1058.58 1287.39 26.02 o 2 4 0 3.03 25.24 10.72 o 3 4 0 9247.39 9305.01 131.93 o 4 4 0 16300.18 16633.54 280.60 o 5 4 0 2362.96 2378.08 51.67 o 6 4 0 1778.94 1614.91 49.35 o 7 4 0 1237.78 1257.72 44.44 o 8 4 0 2600.83 2498.20 84.19 o 9 4 0 222.92 267.99 44.15 o 10 4 0 1698.03 1985.14 130.47 o 11 4 0 154.10 367.05 105.42 o -15 5 0 1298.08 1890.42 244.52 o -14 5 0 38.14 177.36 62.42 o -13 5 0 1512.24 1236.42 115.64 o -12 5 0 373.03 313.35 62.58 o -11 5 0 7793.48 7533.88 210.93 o -10 5 0 970.06 833.43 40.01 o -9 5 0 8760.53 8619.77 173.12 o -8 5 0 100.81 218.10 27.37 o -7 5 0 8786.15 7948.30 134.82 o -6 5 0 230.46 252.02 23.17 o -5 5 0 29571.22 28930.22 495.18 o -4 5 0 3516.81 4047.03 77.45 o -3 5 0 895.45 797.74 22.50 o -2 5 0 1118.51 1101.04 29.43 o -1 5 0 49544.55 51011.84 958.93 o 0 5 0 24667.92 24522.24 487.83 o 1 5 0 745.27 867.80 27.82 o 2 5 0 4653.87 4400.53 68.96 o 3 5 0 19373.54 20053.87 360.76 o 4 5 0 20178.12 21074.38 344.58 o 5 5 0 1101.08 1127.21 43.55 o 6 5 0 720.22 743.77 41.84 o 7 5 0 3642.21 3759.10 99.91 o 8 5 0 10171.26 10899.59 303.61 o 9 5 0 534.49 519.78 68.65 o 10 5 0 130.85 31.35 66.59 o 11 5 0 1066.48 1161.42 175.78 o -15 6 0 4802.43 5129.60 502.38 o -14 6 0 893.80 664.94 157.70 o -13 6 0 559.27 578.95 64.68 o -12 6 0 9771.55 9968.85 309.54 o -11 6 0 16836.38 17662.07 453.81 o -10 6 0 4354.86 4520.76 118.93 o -9 6 0 34.68 100.69 25.46 o -8 6 0 9508.90 9193.04 172.22 o -7 6 0 41272.50 41235.27 815.63 o -6 6 0 7075.08 7048.63 121.11 o -5 6 0 2213.23 2141.52 62.95 o -4 6 0 4946.37 4802.71 95.45 o -3 6 0 31961.66 32327.30 604.53 o -2 6 0 3615.88 3617.36 67.53 o -1 6 0 32.91 62.74 18.51 o 0 6 0 64.96 123.29 28.58 o 1 6 0 14024.68 13900.29 245.66 o 2 6 0 3073.64 3200.40 60.22 o 3 6 0 120.49 111.64 22.86 o 4 6 0 1833.16 2005.63 50.63 o 5 6 0 4071.25 3853.57 92.35 o 6 6 0 3856.81 3529.20 90.47 o 7 6 0 2197.41 2409.92 78.74 o 8 6 0 2478.96 2534.63 97.57 o 9 6 0 205.53 67.37 65.43 o 10 6 0 442.08 434.69 114.97 o -16 7 0 492.17 149.03 185.16 o -15 7 0 463.91 473.11 118.68 o -14 7 0 290.39 175.18 85.47 o -13 7 0 470.57 480.18 51.68 o -12 7 0 4448.19 4088.76 135.56 o -11 7 0 7250.42 7589.16 204.27 o -10 7 0 1178.93 1002.91 45.15 o -9 7 0 1341.27 1340.55 51.29 o -8 7 0 6629.68 6510.49 132.90 o -7 7 0 23644.44 23697.34 468.18 o -6 7 0 862.54 934.45 32.39 o -5 7 0 227.57 158.94 24.53 o -4 7 0 7940.88 7030.37 133.12 o -3 7 0 14973.57 14493.96 303.79 o -2 7 0 6793.05 7431.31 129.88 o -1 7 0 1679.76 1924.04 42.66 o 0 7 0 4275.85 4094.77 82.52 o 1 7 0 22175.27 22117.93 438.91 o 2 7 0 6693.70 6766.21 122.38 o 3 7 0 77.34 89.83 27.93 o 4 7 0 1005.23 1019.58 42.25 o 5 7 0 8765.53 9056.10 207.37 o 6 7 0 5530.40 5469.58 149.90 o 7 7 0 3.67 17.51 30.28 o 8 7 0 74.40 38.10 70.95 o 9 7 0 2595.23 2566.63 289.74 o -16 8 0 109.94 -145.51 168.70 o -15 8 0 749.21 714.96 181.39 o -14 8 0 6831.68 6926.03 434.00 o -13 8 0 5568.90 5642.97 219.31 o -12 8 0 77.96 99.09 42.57 o -11 8 0 59.51 46.97 49.62 o -10 8 0 15617.82 15170.93 346.85 o -9 8 0 19408.06 20222.23 456.15 o -8 8 0 158.92 166.54 38.55 o -7 8 0 296.24 375.74 29.06 o -6 8 0 5460.96 4985.33 120.78 o -5 8 0 17451.24 17570.31 403.09 o -4 8 0 25.43 48.17 19.68 o -3 8 0 620.84 543.49 30.12 o -2 8 0 1165.82 1202.68 37.17 o -1 8 0 6435.73 6191.41 127.91 o 0 8 0 69.24 85.85 17.86 o 1 8 0 3523.14 3369.96 77.75 o 2 8 0 47.40 39.33 14.83 o 3 8 0 1593.09 1465.69 69.04 o 4 8 0 431.74 419.36 57.20 o 5 8 0 2409.17 2733.97 111.71 o 6 8 0 799.90 754.65 70.08 o 7 8 0 580.51 433.68 97.10 o 8 8 0 166.36 -10.59 101.44 o -16 9 0 623.18 747.85 320.51 o -15 9 0 80.23 9.09 134.20 o -14 9 0 3959.49 3601.08 219.25 o -13 9 0 1069.42 1037.71 70.06 o -12 9 0 833.86 901.55 54.04 o -11 9 0 1370.76 1431.24 61.10 o -10 9 0 14219.30 14311.03 395.28 o -9 9 0 10424.87 10588.80 292.53 o -8 9 0 45.60 97.24 27.96 o -7 9 0 27.13 1.96 30.53 o -6 9 0 4594.17 4409.56 102.95 o -5 9 0 21425.88 21198.42 508.86 o -4 9 0 1003.94 1162.82 38.11 o -3 9 0 86.97 90.47 22.83 o -2 9 0 8677.68 8307.74 181.74 o -1 9 0 9328.21 9400.69 185.69 o 0 9 0 198.82 200.11 25.22 o 1 9 0 566.86 581.52 36.16 o 2 9 0 7408.76 7383.48 177.48 o 3 9 0 9270.12 9224.32 264.59 o 4 9 0 1531.37 1617.15 86.02 o 5 9 0 715.77 721.07 83.39 o 6 9 0 260.32 105.31 98.18 o 7 9 0 2928.43 3107.53 331.53 o -15 10 0 752.19 723.83 202.27 o -14 10 0 179.32 -19.39 86.28 o -13 10 0 1057.87 1050.48 83.84 o -12 10 0 9086.59 9139.95 327.48 o -11 10 0 1335.37 1246.92 61.45 o -10 10 0 3049.21 2937.47 94.91 o -9 10 0 46.53 43.15 28.11 o -8 10 0 7549.82 7287.94 206.14 o -7 10 0 2423.41 2264.63 71.66 o -6 10 0 99.14 153.11 25.21 o -5 10 0 686.18 634.73 33.99 o -4 10 0 619.36 629.50 28.70 o -3 10 0 1471.98 1458.83 51.33 o -2 10 0 1148.47 1207.66 42.73 o -1 10 0 1792.38 1609.54 51.58 o 0 10 0 2096.86 2182.97 66.40 o 1 10 0 1166.13 1110.66 46.87 o 2 10 0 4367.31 4458.86 157.19 o 3 10 0 4717.99 4756.31 187.29 o 4 10 0 40.70 -27.28 99.11 o 5 10 0 406.84 377.33 76.52 o 6 10 0 146.53 202.64 160.70 o -15 11 0 72.42 -52.53 107.40 o -14 11 0 463.48 529.60 94.78 o -13 11 0 1287.00 1261.28 86.99 o -12 11 0 8595.35 9007.67 338.73 o -11 11 0 3587.35 3367.55 130.70 o -10 11 0 122.47 182.21 46.90 o -9 11 0 1325.39 1445.55 78.91 o -8 11 0 9964.66 10470.06 297.55 o -7 11 0 9633.11 9292.90 260.03 o -6 11 0 344.73 377.05 30.13 o -5 11 0 38.72 1.55 27.73 o -4 11 0 10702.36 11185.67 264.59 o -3 11 0 2508.14 2439.97 76.38 o -2 11 0 69.51 72.46 27.52 o -1 11 0 12.98 93.01 31.97 o 0 11 0 4512.22 4796.71 152.15 o 1 11 0 4649.14 4725.13 148.43 o 2 11 0 40.62 77.32 47.68 o 3 11 0 153.87 99.14 57.78 o 4 11 0 1037.80 828.35 115.49 o 5 11 0 3105.89 3968.63 554.16 o -15 12 0 1268.50 1116.62 194.29 o -14 12 0 2554.03 2441.04 221.48 o -13 12 0 23.26 0.49 59.97 o -12 12 0 1152.12 1207.62 76.74 o -11 12 0 405.65 270.81 48.21 o -10 12 0 3654.13 3317.09 126.86 o -9 12 0 457.49 632.51 63.26 o -8 12 0 2676.98 2745.51 95.49 o -7 12 0 40.15 33.02 34.92 o -6 12 0 523.07 678.41 48.66 o -5 12 0 433.83 476.96 28.98 o -4 12 0 2485.60 2371.71 74.11 o -3 12 0 1042.62 977.75 47.77 o -2 12 0 166.94 86.67 49.30 o -1 12 0 23.48 -34.70 57.41 o 0 12 0 3008.01 2765.29 105.14 o 1 12 0 3111.31 2788.24 160.44 o 2 12 0 438.23 331.53 79.10 o 3 12 0 310.78 483.35 119.10 o 4 12 0 1354.66 992.60 194.20 o -14 13 0 2797.77 2868.93 347.03 o -13 13 0 94.32 151.77 69.46 o -12 13 0 12.10 -11.22 87.17 o -11 13 0 3446.99 3394.06 182.00 o -10 13 0 6506.33 6536.50 258.14 o -9 13 0 1524.32 1357.98 71.20 o -8 13 0 50.32 20.77 56.09 o -7 13 0 2074.88 2403.42 92.70 o -6 13 0 7762.71 7543.76 226.42 o -5 13 0 2088.98 1980.00 87.42 o -4 13 0 6.64 25.05 33.82 o -3 13 0 1408.71 1602.52 79.40 o -2 13 0 3785.72 4043.13 154.53 o -1 13 0 1024.19 818.02 72.57 o 0 13 0 160.73 141.75 80.92 o 1 13 0 3.56 -87.86 101.94 o 2 13 0 2493.04 2975.95 305.27 o -13 14 0 573.40 824.36 123.96 o -12 14 0 488.28 62.03 87.19 o -11 14 0 131.43 -54.68 83.94 o -10 14 0 730.77 740.48 68.64 o -9 14 0 10.25 66.82 43.80 o -8 14 0 394.28 474.20 73.89 o -7 14 0 392.87 453.56 54.59 o -6 14 0 1478.48 1533.79 79.42 o -5 14 0 43.00 -24.36 38.61 o -4 14 0 942.20 1001.09 91.75 o -3 14 0 561.56 549.29 72.87 o -2 14 0 3086.89 2815.56 193.16 o -1 14 0 1056.94 956.80 124.50 o 0 14 0 106.54 87.01 96.36 o 1 14 0 25.11 46.21 131.80 o -12 15 0 2427.73 2266.68 229.60 o -11 15 0 65.21 -23.02 78.64 o -10 15 0 157.81 4.92 163.00 o -9 15 0 1993.09 2045.63 150.99 o -8 15 0 2775.56 2771.14 179.84 o -7 15 0 280.74 314.19 60.45 o -6 15 0 26.44 -70.07 70.07 o -5 15 0 1622.35 1746.89 146.34 o -4 15 0 4334.34 4045.53 292.37 o -3 15 0 414.64 137.77 61.84 o -2 15 0 32.43 -33.73 116.82 o -1 15 0 344.66 354.47 238.88 o -11 16 0 147.52 397.52 125.78 o -10 16 0 57.82 -94.20 94.20 o -9 16 0 1228.20 1222.02 205.12 o -8 16 0 1345.29 1198.66 145.92 o -7 16 0 5.01 80.42 88.72 o -6 16 0 19.11 -15.08 89.53 o -5 16 0 1066.85 1198.20 187.68 o -4 16 0 2218.46 2221.48 283.33 o 4 -16 1 1.12 -93.36 93.36 o 5 -16 1 96.15 205.81 74.74 o 6 -16 1 2032.78 2424.09 223.35 o 7 -16 1 606.56 878.82 117.82 o 8 -16 1 1.47 -79.93 79.93 o 9 -16 1 14.80 133.92 126.65 o 10 -16 1 1166.79 899.70 153.33 o 11 -16 1 698.76 710.98 213.46 o 1 -15 1 422.93 537.60 356.11 o 2 -15 1 1978.82 2056.26 199.94 o 3 -15 1 3.99 -72.57 72.57 o 4 -15 1 85.82 33.87 67.87 o 5 -15 1 264.76 54.54 79.59 o 6 -15 1 2290.85 2300.93 178.59 o 7 -15 1 429.20 701.77 134.59 o 8 -15 1 77.47 170.01 82.98 o 9 -15 1 826.79 857.49 96.73 o 10 -15 1 2330.67 2167.79 184.43 o 11 -15 1 2289.56 2362.43 197.83 o 12 -15 1 13.80 54.23 93.31 o -1 -14 1 2104.12 1924.79 310.27 o 0 -14 1 2577.73 2794.70 301.82 o 1 -14 1 32.88 -64.51 68.29 o 2 -14 1 39.84 73.40 50.25 o 3 -14 1 2348.01 2159.92 143.35 o 4 -14 1 3433.36 3430.32 172.21 o 5 -14 1 140.92 161.78 70.21 o 6 -14 1 239.12 333.84 53.54 o 7 -14 1 430.51 486.02 90.12 o 8 -14 1 1938.79 1925.45 112.69 o 9 -14 1 14.39 57.55 61.37 o 10 -14 1 334.14 178.89 54.69 o 11 -14 1 113.37 95.53 54.32 o 12 -14 1 1632.08 1591.78 145.44 o 13 -14 1 76.73 140.35 113.14 o -3 -13 1 411.63 636.71 205.71 o -2 -13 1 293.68 389.11 249.65 o -1 -13 1 1860.63 1588.99 170.90 o 0 -13 1 2588.12 3166.93 243.48 o 1 -13 1 17.23 87.84 42.65 o 2 -13 1 286.69 184.21 43.56 o 3 -13 1 6106.99 6319.13 221.61 o 4 -13 1 4785.24 5137.13 169.91 o 5 -13 1 559.31 591.08 47.86 o 6 -13 1 131.22 103.22 44.06 o 7 -13 1 4275.47 4097.17 143.57 o 8 -13 1 5733.86 5691.60 199.53 o 9 -13 1 605.32 700.24 61.36 o 10 -13 1 102.96 56.33 46.31 o 11 -13 1 2893.26 2632.77 144.75 o 12 -13 1 6523.00 6629.87 398.19 o 13 -13 1 1393.16 1510.32 144.22 o 14 -13 1 5.13 43.71 105.36 o -4 -12 1 385.05 489.24 144.49 o -3 -12 1 3126.22 3208.21 332.92 o -2 -12 1 2863.16 3123.46 176.09 o -1 -12 1 14.69 21.24 81.55 o 0 -12 1 136.04 135.93 47.68 o 1 -12 1 4896.06 4599.92 150.66 o 2 -12 1 2202.14 2418.47 88.88 o 3 -12 1 5.33 -4.81 36.00 o 4 -12 1 182.38 127.09 28.29 o 5 -12 1 4943.69 4820.29 135.64 o 6 -12 1 4357.43 4519.56 126.49 o 7 -12 1 392.59 360.03 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