[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m50-m51
[ doi:10.1107/S1600536812050155 ]

Hexakis([mu]3-2-hydroxynaphthalene-1-carboxaldehyde thiosemicarbazonato-[kappa]3N2:S:S)hexasilver(I) N,N-dimethylformamide tetrasolvate

Q. Sun, L. Chai, H. Liu and J. Wang


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.16 PLAT230_ALERT_2_C Hirshfeld Test Diff for C25 -- C26 .. 6.3 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ag1 -- S1 .. 5.6 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Ag1 -- S3_a .. 5.8 su PLAT234_ALERT_4_C Large Hirshfeld Difference C31 -- C32 .. 0.16 Ang. PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C30 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.192 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 68 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 3 PLAT975_ALERT_2_C Positive Residual Density at 0.92A from O6 . 0.68 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.69A from O6 . 0.68 eA-3
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 12 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 9 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N10 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N11 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N12 PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of N13 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT335_ALERT_2_G Check Large C6 Ring C-C Range C25 -C34 0.15 Ang. PLAT335_ALERT_2_G Check Large C6 Ring C-C Range C28 -C33 0.19 Ang. PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C43 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C44 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C46 PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C47 PLAT764_ALERT_4_G Overcomplete CIF Bond List Detected (Rep/Expd) . 1.10 Ratio PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms .... ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 63 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 57 Perc. PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 12 ALERT level C = Check. Ensure it is not caused by an omission or oversight 23 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 11 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 11 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster