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Acta Cryst. (2013). E69, m68-m69
[ doi:10.1107/S1600536812050970 ]

Bis[[mu]-bis(diphenylphosphanyl)methane-[kappa]2P:P']([mu]-1-ethylthiourea-[kappa]2S:S)bis[iodidocopper(I)] acetonitrile sesquisolvate

R. Nimthong, Y. Wattanakanjana and C. Pakawatchai


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT911_ALERT_3_B Missing # FCF Refl Between THmin & STh/L= 0.600 2851 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.9 Ratio PLAT480_ALERT_4_C Long H...A H-Bond Reported H63 .. S1 .. 2.95 Ang. PLAT481_ALERT_4_C Long D...A H-Bond Reported C14 .. CG1 .. 4.08 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 41 A   3 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 6.211 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 5 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT045_ALERT_1_G Calculated and Reported Z Differ by ............ 0.50 Ratio PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) I1 -- Cu1 .. 9.0 su PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of C8 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 33 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 3 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 371
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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