[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m75-m76
[ doi:10.1107/S1600536812051999 ]

cis-Bis(1,10-phenanthroline-[kappa]2N,N')bis(pyridin-4-amine-[kappa]N1)ruthenium(II) bis(hexafluoridophosphate)

M. R. Camilo, F. T. Martins, V. R. S. Malta, J. Ellena and R. M. Carlos


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for C5 -- C6 .. 5.2 su PLAT234_ALERT_4_C Large Hirshfeld Difference C3 -- C4 .. 0.20 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C7 -- C8 .. 0.16 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C8 -- C9 .. 0.16 Ang. PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C2 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C5 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C8 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C9A PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of P1 PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of P1A PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.5 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0112 Ang PLAT420_ALERT_2_C D-H Without Acceptor N4 - H4B ... ? PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.266 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 67 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 42
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 4 PLAT128_ALERT_4_G Alternate Setting of Space-group Pna21 ....... P21cn PLAT335_ALERT_2_G Check Large C6 Ring C-C Range C4 -C12 0.15 Ang. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 2 PLAT917_ALERT_2_G The FCF is likely NOT based on a BASF/TWIN Flack !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 17 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 9 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 7 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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