Acta Cryst. (2013). E69, o273-o274
[ doi:10.1107/S160053681300144X ]
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Alert level C PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.56 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.891 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6
Alert level G REFLT03_ALERT_1_G ALERT: Expected hkl max differ from CIF values From the CIF: _diffrn_reflns_theta_max 36.92 From the CIF: _reflns_number_total 13130 From the CIF: _diffrn_reflns_limit_ max hkl 20. 28. 41. From the CIF: _diffrn_reflns_limit_ min hkl -20. -27. -41. TEST1: Expected hkl limits for theta max Calculated maximum hkl 20. 28. 46. Calculated minimum hkl -20. -28. -46. PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 2 PLAT063_ALERT_4_G Crystal Size Likely too Large for Beam Size .... 0.64 mm PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 6 PLAT793_ALERT_4_G The Model has Chirality at C7A (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C7B (Verify) .... S PLAT793_ALERT_4_G The Model has Chirality at C8A (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C8B (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C9A (Verify) .... R PLAT793_ALERT_4_G The Model has Chirality at C9B (Verify) .... R PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 846 PLAT952_ALERT_5_G Reported and Calculated Lmax Values Differ by .. 5
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 13 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 9 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check
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Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
|Author Response: Horak the synthesis of 5-oxo-6-phenyl-4a,5,6,7,7a,8-hexahydro-4H-furo[2,3- f]isoindole-4-carboxylic acid by the reaction of 3-(2-furyl)-2- propenyl(phenyl)amine with maleic anhydride. The development of cycloaddition reaction conditions.|
Lytvyn spectral investigation, 1? and 13? NMR spectra interpretation. The establishment of the reaction stereochemistry. Zubkov development of reduction method and the synthesis of 3-(2-furyl)-2- propenyl(phenyl)amine. Nikitina the synthesis of phenyl-(E)-3-(2-furyl)-2-propen-1-imine by the reaction of 3-(2-furyl)-2-propenal with aniline. Homza the synthesis of 3-(2-furyl)-2-propenal. Lis - crystallographic investigation. Kinzhybalo - crystallographic investigation. Obushak supervisor of the investigation, the search and analysis of literatur sources on the topic. .
1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing
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