[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m88
[ doi:10.1107/S1600536812051707 ]

Tetrabromido[4-(triphenylphosphanyloxy)butyl]tellurium acetonitrile monosolvate

S. M. Närhi, R. Oilunkaniemi and R. S. Laitinen


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low ....... 0.941 PLAT911_ALERT_3_B Missing # FCF Refl Between THmin & STh/L= 0.595 293 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 2
Alert level C REFLT03_ALERT_3_C Reflection count < 95% complete From the CIF: _diffrn_reflns_theta_max 25.00 From the CIF: _diffrn_reflns_theta_full 25.00 From the CIF: _reflns_number_total 4684 TEST2: Reflns within _diffrn_reflns_theta_max Count of symmetry unique reflns 4980 Completeness (_total/calc) 94.06% PLAT244_ALERT_4_C Low 'Solvent' Ueq as Compared to Neighbors of C5 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0112 Ang PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 8.11 PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 C2 H3 N PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 59 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster