Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 2 (February 2013)


organic compounds



nc2302 scheme

Acta Cryst. (2013). E69, o229    [ doi:10.1107/S1600536813000494 ]

2-Chloro-N-methyl-N-[2-(methylamino)phenyl]acetamide

Y.-B. Bai, X.-H. Chen, Y.-T. Ma, A.-L. Zhang and J.-M. Gao

Abstract: The title compound, C10H13ClN2O, was obtained as a by-product in the reaction of 2-chloromethyl-1H-benzimidazole, dimethyl sulfate and toluene to synthesise 2-chloromethyl-1-methylbenzimidazole. The dihedral angle between the benzene ring and the acetamide group is 89.72  (6)° while that between the aromatic ring and the chloracetyl group is 84.40 (4)°. In the crystal, adjacent molecules are linked by pairs of N-H...O hydrogen bonds into inversion dimers.


htmldisplay filedownload file

Hyper-Text Markup Language (HTML) file
[ doi:10.1107/S1600536813000494/nc2302sup0.html ]
Supplementary materials


cdxdisplay filedownload file

Chemdraw file (1.9 kbytes)
[ doi:10.1107/S1600536813000494/nc2302Isup4.cdx ]
Supplementary material


cmldisplay filedownload file

Chemical Markup Language (CML) file (4.1 kbytes)
[ doi:10.1107/S1600536813000494/nc2302Isup4.cml ]
Supplementary material


Notes:

To open or display or play some files, you may need to set your browser up to use the appropriate software. See the full list of file types for an explanation of the different file types and their related mime types and, where available links to sites from where the appropriate software may be obtained.

The download button will force most browsers to prompt for a file name to store the data on your hard disk.

Where possible, images are represented by thumbnails.

 bibliographic record in  format

  Find reference:   Volume   Page   
  Search:     From   to      Advanced search

Copyright © International Union of Crystallography
IUCr Webmaster