[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m73-m74
[ doi:10.1107/S1600536812051422 ]

Di-[mu]-chlorido-bis[(2,2'-bipyridine-5,5'-dicarboxylic acid-[kappa]2N,N')chloridocopper(II)] dimethylformamide tetrasolvate

S. Øien, D. S. Wragg, K. P. Lillerud and M. Tilset


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT480_ALERT_4_C Long H...A H-Bond Reported H21A .. O2 .. 2.71 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H21B .. O1 .. 2.72 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 66
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 3 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00600 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- Cl2 .. 11.0 su PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 20 Perc. PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 3 C3 H7 N O PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 201
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 5 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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