[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m125
[ doi:10.1107/S1600536813002274 ]

catena-Poly[[bis([mu]2-1,4,7,10,13,16-hexaoxacyclooctadecane)dipotassium]-[mu]2-iodido-(iodidocadmium)-di-[mu]2-iodido-(iodidocadmium)-[mu]2-iodido]

K. Rajarajan, A. Pugazhenthi and M. NizamMohideen


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C3 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C4 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0094 Ang PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C3 - C4 ... 1.35 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 2 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 7.12 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) I1 -- Cd1 .. 16.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) I1 -- Cd1_a .. 11.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) I3 -- Cd1 .. 7.0 su PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 4 Perc. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 2 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 6 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 77 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 13 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster