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[Contents scheme]

Acta Cryst. (2013). E69, m121
[ doi:10.1107/S160053681300158X ]

{Bis[N,N'-dicyclohexyl-N'',N''-bis(trimethylsilyl)guanidinato-[kappa]2N,N']neodymium(III)}di-[mu]-chlorido-[bis(tetrahydrofuran-[kappa]O)lithium]

S.-H. Chi and J. Chen


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 19 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for O2 -- C43 .. 5.5 su PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C41 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Si2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Si3 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0081 Ang PLAT723_ALERT_1_C Torsion Calc 178.8(13), Rep 18.00 Dev... 160.80 Sigma SI3 -N6 -C20 -ND1 1.555 1.555 1.555 1.555 165 PLAT743_ALERT_1_C Torsion Calc 178.8(13), Rep 18.00 ...... Missing su SI3 -N6 -C20 -ND1 1.555 1.555 1.555 1.555 165 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 6.969 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 17
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 4 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Nd1 -- Cl2 .. 5.5 su PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 3 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 4 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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