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[Contents scheme]

Acta Cryst. (2013). E69, m124
[ doi:10.1107/S1600536813000585 ]

catena-Poly[[[triaqua[3-(4-carboxyphenoxy)phthalato-[kappa]O2]manganese(II)]-[mu]-4,4'-bipyridine-[kappa]2N:N'] 4,4'-bipyridine monosolvate dihydrate]

W. Sun


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C28 PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1 C25 H22 Mn N2 O10 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 71
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 15 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 3 PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 11 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Mn1 -- O8 .. 6.7 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Mn1 -- O9 .. 6.9 su PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 18 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 50 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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