# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' apx710 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 652.75 _exptl_crystal_F_000 3592.00 _reflns_d_resolution_high 0.8297 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 11.8871 _cell_length_b 31.8243 _cell_length_c 18.5168 _cell_angle_alpha 90.000 _cell_angle_beta 95.880 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 165870.69 180683.23 7616.82 o 3 0 0 9014.01 8356.81 424.92 o 4 0 0 107086.12 106700.41 4574.03 o 5 0 0 17972.54 16857.43 827.80 o 6 0 0 111933.45 113490.20 4907.51 o 7 0 0 15.64 92.14 150.66 o 8 0 0 3226.55 3525.12 464.66 o 9 0 0 7043.36 8587.37 639.05 o 10 0 0 61.24 -176.65 176.65 o 11 0 0 14067.70 15378.20 944.22 o 12 0 0 176.20 589.79 372.14 o 13 0 0 1219.30 543.70 316.87 o 14 0 0 2260.66 2396.30 626.31 o 1 1 0 31134.99 32992.43 1228.29 o 2 1 0 38260.43 41304.73 1260.54 o 3 1 0 6898.28 6856.43 256.02 o 4 1 0 355.86 380.64 62.49 o 5 1 0 7789.89 7582.00 396.29 o 6 1 0 5542.14 5551.59 260.32 o 7 1 0 822.56 472.96 120.86 o 8 1 0 1901.01 2395.78 217.48 o 9 1 0 4259.67 4296.93 301.16 o 10 1 0 9123.32 9337.72 462.91 o 11 1 0 139.05 75.25 180.58 o 12 1 0 40.73 38.88 161.29 o 13 1 0 123.44 -84.97 207.64 o 14 1 0 866.92 479.96 507.95 o 1 2 0 87546.02 89056.02 3266.20 o 2 2 0 39240.68 41352.13 1164.64 o 3 2 0 571.89 729.17 83.15 o 4 2 0 9148.81 8315.97 288.64 o 5 2 0 2630.62 3084.04 182.24 o 6 2 0 424.50 519.79 85.80 o 7 2 0 19940.22 19076.15 823.48 o 8 2 0 13878.85 13815.33 610.72 o 9 2 0 3887.02 3608.46 311.95 o 10 2 0 86.88 25.84 154.97 o 11 2 0 2056.93 1314.21 206.62 o 12 2 0 6397.76 6377.51 436.13 o 13 2 0 7640.77 8316.58 583.95 o 14 2 0 31.11 210.22 292.41 o 1 3 0 33756.81 35645.39 1189.16 o 2 3 0 32720.26 34395.09 978.07 o 3 3 0 48047.09 48785.73 1384.16 o 4 3 0 4234.97 4854.58 196.04 o 5 3 0 7292.93 6968.87 268.51 o 6 3 0 1239.84 1343.14 126.36 o 7 3 0 347.72 620.36 100.40 o 8 3 0 8716.02 8421.81 401.09 o 9 3 0 638.79 328.69 156.52 o 10 3 0 177.21 233.77 135.06 o 11 3 0 9884.67 10428.54 530.75 o 12 3 0 136.59 45.91 233.75 o 13 3 0 3165.63 2800.00 385.08 o 14 3 0 1166.83 325.08 246.25 o 0 4 0 31793.13 33156.73 1760.39 o 1 4 0 12439.29 12278.76 336.92 o 2 4 0 14218.81 15123.25 395.96 o 3 4 0 296.56 361.75 60.52 o 4 4 0 1273.72 1197.89 143.17 o 5 4 0 10756.23 10090.06 357.26 o 6 4 0 11.11 -62.59 63.69 o 7 4 0 443.15 248.51 92.63 o 8 4 0 40646.59 38842.78 1371.74 o 9 4 0 5054.00 4908.94 296.42 o 10 4 0 7217.88 7904.41 528.40 o 11 4 0 4758.87 4746.11 358.69 o 12 4 0 256.58 289.39 258.69 o 13 4 0 1895.97 1689.76 339.65 o 14 4 0 8015.71 9229.30 950.40 o 1 5 0 59655.66 60003.14 1561.66 o 2 5 0 8818.49 8807.16 262.31 o 3 5 0 0.01 -25.08 40.60 o 4 5 0 1340.19 1230.44 102.16 o 5 5 0 9.64 165.67 87.95 o 6 5 0 793.28 640.84 99.56 o 7 5 0 1187.64 989.71 165.06 o 8 5 0 620.99 744.40 152.14 o 9 5 0 15402.92 14903.32 615.59 o 10 5 0 18574.65 18464.12 939.38 o 11 5 0 1303.48 1418.67 319.33 o 12 5 0 15.66 9.79 233.78 o 13 5 0 106.81 214.42 257.10 o 14 5 0 291.24 117.41 288.77 o 0 6 0 45027.34 50268.46 1868.38 o 1 6 0 1851.04 1724.67 77.87 o 2 6 0 13035.46 12264.97 351.44 o 3 6 0 5311.89 5456.91 190.00 o 4 6 0 5205.44 5937.03 230.50 o 5 6 0 6.22 -39.08 69.86 o 6 6 0 13599.23 13123.21 451.79 o 7 6 0 7163.80 7077.55 312.37 o 8 6 0 91.46 22.69 113.33 o 9 6 0 2263.32 2148.35 299.17 o 10 6 0 1.03 40.70 217.93 o 11 6 0 183.91 -104.31 201.13 o 12 6 0 5441.36 5384.32 446.05 o 13 6 0 3197.69 3341.42 412.19 o 14 6 0 110.15 263.63 314.12 o 1 7 0 535.44 687.16 56.13 o 2 7 0 10331.19 10812.52 333.37 o 3 7 0 33503.95 32047.21 874.29 o 4 7 0 5580.71 6151.15 220.40 o 5 7 0 8173.79 8355.51 289.18 o 6 7 0 19636.02 20463.49 656.38 o 7 7 0 11438.58 11212.13 428.49 o 8 7 0 46379.55 48544.19 1581.35 o 9 7 0 6286.59 5535.39 407.59 o 10 7 0 6253.01 6667.16 441.77 o 11 7 0 4875.56 3921.88 530.00 o 12 7 0 3486.20 3331.20 372.60 o 13 7 0 739.30 1165.85 321.92 o 14 7 0 6497.37 7708.92 953.64 o 0 8 0 2645.87 3095.21 173.35 o 1 8 0 31970.21 32377.79 872.67 o 2 8 0 13739.86 14627.92 445.39 o 3 8 0 276.65 315.06 61.17 o 4 8 0 174.63 142.32 60.10 o 5 8 0 526.42 711.69 84.99 o 6 8 0 9830.10 9241.38 316.41 o 7 8 0 4464.78 4165.07 241.99 o 8 8 0 8.57 226.78 115.52 o 9 8 0 5781.05 5983.52 346.94 o 10 8 0 6092.88 6167.21 552.64 o 11 8 0 368.64 200.58 255.03 o 12 8 0 966.92 767.79 259.11 o 13 8 0 2337.18 1971.10 373.50 o 1 9 0 61390.55 60123.41 1585.14 o 2 9 0 416.06 457.08 59.68 o 3 9 0 276.83 421.45 77.85 o 4 9 0 8137.56 8145.95 284.30 o 5 9 0 10469.43 10625.38 353.51 o 6 9 0 31138.40 30820.05 876.45 o 7 9 0 3286.78 3565.69 218.55 o 8 9 0 6775.90 7055.12 376.42 o 9 9 0 573.58 553.73 220.02 o 10 9 0 7145.70 7442.37 474.82 o 11 9 0 917.03 620.34 279.32 o 12 9 0 2409.57 2177.75 375.23 o 13 9 0 82.16 4.40 288.52 o 0 10 0 1793.68 1971.71 141.01 o 1 10 0 18.95 -41.78 41.78 o 2 10 0 423.57 420.59 62.67 o 3 10 0 6572.68 6684.02 230.98 o 4 10 0 2117.29 2083.64 124.84 o 5 10 0 28503.85 28024.19 799.33 o 6 10 0 857.41 881.63 99.19 o 7 10 0 11743.95 12275.15 461.59 o 8 10 0 6120.85 6610.45 357.15 o 9 10 0 11654.88 11663.02 583.88 o 10 10 0 2357.83 2608.48 291.73 o 11 10 0 413.45 554.48 253.66 o 12 10 0 687.61 505.27 271.94 o 13 10 0 392.41 191.20 276.38 o 1 11 0 3645.92 4016.42 210.05 o 2 11 0 34.41 0.95 73.40 o 3 11 0 9653.28 10410.20 329.73 o 4 11 0 1266.60 1209.98 102.97 o 5 11 0 7260.41 7811.42 282.93 o 6 11 0 128.80 197.39 87.32 o 7 11 0 1482.62 1665.18 165.34 o 8 11 0 3791.15 3844.48 376.21 o 9 11 0 10022.79 9208.93 499.87 o 10 11 0 25.24 58.47 175.10 o 11 11 0 1067.92 845.33 252.37 o 12 11 0 1653.09 1735.57 395.90 o 13 11 0 17.16 61.13 347.02 o 0 12 0 29.50 104.77 118.40 o 1 12 0 2632.49 2679.76 137.56 o 2 12 0 105.60 45.85 52.56 o 3 12 0 51415.12 51869.81 1403.40 o 4 12 0 4817.25 4733.35 223.51 o 5 12 0 22162.52 23091.63 674.16 o 6 12 0 5333.81 4958.14 384.89 o 7 12 0 12447.77 12245.92 505.71 o 8 12 0 121.90 278.32 128.81 o 9 12 0 15902.53 14608.23 736.71 o 10 12 0 1069.36 917.36 222.98 o 11 12 0 2285.39 1776.71 283.92 o 12 12 0 87.00 1.81 216.10 o 13 12 0 451.83 347.85 251.98 o 1 13 0 346.79 296.80 61.72 o 2 13 0 2026.08 2364.19 162.19 o 3 13 0 2058.99 2216.35 127.75 o 4 13 0 2423.15 2145.18 132.15 o 5 13 0 2192.64 2385.82 147.54 o 6 13 0 1456.37 1584.29 144.38 o 7 13 0 5582.80 5596.79 310.77 o 8 13 0 1066.66 1453.08 244.58 o 9 13 0 4452.75 4934.05 488.85 o 10 13 0 20.10 -99.94 170.62 o 11 13 0 8.42 21.69 208.30 o 12 13 0 814.00 842.73 258.89 o 13 13 0 1687.80 1700.75 306.09 o 0 14 0 41956.03 44461.75 1710.53 o 1 14 0 20689.49 21461.10 618.23 o 2 14 0 55816.55 56971.65 1535.39 o 3 14 0 2147.46 1997.98 141.99 o 4 14 0 3630.44 4225.01 191.36 o 5 14 0 1170.91 1054.92 111.85 o 6 14 0 4210.59 4597.92 273.98 o 7 14 0 5878.79 6126.90 334.89 o 8 14 0 10167.17 9816.32 533.84 o 9 14 0 2194.48 2548.83 279.42 o 10 14 0 2090.12 2162.91 281.52 o 11 14 0 430.63 115.21 227.47 o 12 14 0 2769.74 2474.54 337.21 o 13 14 0 521.56 385.29 345.82 o 1 15 0 1084.02 1198.14 98.32 o 2 15 0 15799.54 15428.28 464.49 o 3 15 0 593.25 551.19 79.30 o 4 15 0 2772.91 3224.23 168.07 o 5 15 0 115.29 177.15 99.49 o 6 15 0 4239.85 3768.76 256.07 o 7 15 0 4865.95 5195.70 375.14 o 8 15 0 38.18 159.04 120.23 o 9 15 0 170.61 457.88 179.02 o 10 15 0 748.75 484.63 249.20 o 11 15 0 89.57 254.62 197.63 o 12 15 0 0.55 94.15 305.53 o 13 15 0 560.95 230.18 334.73 o 0 16 0 36917.83 35487.30 1463.79 o 1 16 0 3658.51 4101.60 184.86 o 2 16 0 5472.31 5709.85 306.37 o 3 16 0 5625.92 5848.37 231.61 o 4 16 0 102.57 7.98 63.65 o 5 16 0 7891.69 7763.34 404.56 o 6 16 0 20443.51 19503.50 720.19 o 7 16 0 99.30 98.01 123.92 o 8 16 0 1739.10 1813.23 216.92 o 9 16 0 5239.87 4568.25 361.42 o 10 16 0 1793.26 2020.42 287.11 o 11 16 0 2428.35 2380.60 429.02 o 12 16 0 1.07 -238.77 304.15 o 1 17 0 478.19 458.76 79.32 o 2 17 0 3651.91 3518.98 169.94 o 3 17 0 5896.84 6448.61 253.81 o 4 17 0 19186.01 17754.22 594.52 o 5 17 0 1898.71 2055.85 173.70 o 6 17 0 2.90 -101.69 114.22 o 7 17 0 388.22 639.20 156.75 o 8 17 0 603.16 609.13 152.77 o 9 17 0 23.49 322.16 294.84 o 10 17 0 1511.50 2164.53 488.44 o 11 17 0 80.31 389.70 305.81 o 12 17 0 124.84 124.53 328.79 o 0 18 0 914.43 1192.07 201.78 o 1 18 0 6058.44 6228.83 246.78 o 2 18 0 22852.32 23398.68 722.94 o 3 18 0 124.46 28.22 71.12 o 4 18 0 267.43 83.39 113.45 o 5 18 0 542.63 574.27 114.70 o 6 18 0 5660.31 5442.77 316.15 o 7 18 0 4415.39 4706.91 315.91 o 8 18 0 1018.17 1198.75 251.44 o 9 18 0 337.96 213.13 233.43 o 10 18 0 723.87 1083.77 296.25 o 11 18 0 269.97 -65.22 277.58 o 12 18 0 2488.44 1594.62 513.34 o 1 19 0 13894.84 14753.57 466.55 o 2 19 0 8354.70 7350.67 300.32 o 3 19 0 2438.00 2663.85 179.55 o 4 19 0 1126.57 1153.47 137.17 o 5 19 0 3993.45 4471.12 349.59 o 6 19 0 104.27 -56.51 163.96 o 7 19 0 2056.56 1807.57 256.71 o 8 19 0 6356.05 6313.09 433.42 o 9 19 0 577.87 732.91 288.34 o 10 19 0 99.41 109.91 254.35 o 11 19 0 7132.09 6754.41 898.09 o 12 19 0 4280.65 5168.41 938.22 o 0 20 0 5738.45 5867.87 360.71 o 1 20 0 20883.49 19254.44 586.75 o 2 20 0 33821.58 33909.30 961.61 o 3 20 0 1650.90 1888.68 161.97 o 4 20 0 8859.49 8492.49 413.60 o 5 20 0 684.36 463.76 154.71 o 6 20 0 2051.88 2256.80 272.58 o 7 20 0 4264.84 5236.98 397.65 o 8 20 0 8429.04 7891.31 498.58 o 9 20 0 2282.31 2315.44 410.65 o 10 20 0 110.37 434.56 297.01 o 11 20 0 1405.00 1620.17 377.51 o 12 20 0 572.29 553.61 424.47 o 1 21 0 19660.57 19647.22 603.54 o 2 21 0 54.07 68.90 105.54 o 3 21 0 62.36 267.11 130.00 o 4 21 0 13286.05 13484.65 566.40 o 5 21 0 4124.09 4032.12 269.22 o 6 21 0 10893.73 12148.76 670.85 o 7 21 0 2807.05 2607.34 294.44 o 8 21 0 634.52 898.13 233.78 o 9 21 0 3512.46 4097.06 449.42 o 10 21 0 14577.50 14016.85 944.37 o 11 21 0 1131.83 1053.94 362.48 o 0 22 0 8338.74 8359.27 743.72 o 1 22 0 10195.50 11354.19 428.93 o 2 22 0 911.13 887.47 148.12 o 3 22 0 119.76 212.06 172.78 o 4 22 0 2618.17 2579.06 243.39 o 5 22 0 5389.46 5711.23 341.55 o 6 22 0 5254.52 5405.38 513.99 o 7 22 0 3308.20 3171.37 330.26 o 8 22 0 536.13 910.09 285.22 o 9 22 0 4147.26 3632.86 434.32 o 10 22 0 2.23 29.94 369.37 o 11 22 0 4361.23 4494.19 511.66 o 1 23 0 7504.55 7939.87 508.94 o 2 23 0 5258.16 5496.08 328.55 o 3 23 0 37523.69 38824.14 1303.22 o 4 23 0 188.22 143.68 147.28 o 5 23 0 287.38 173.09 153.23 o 6 23 0 3876.64 4638.95 442.85 o 7 23 0 730.63 680.82 229.25 o 8 23 0 17745.19 18100.52 848.34 o 9 23 0 7128.74 7126.26 595.02 o 10 23 0 365.26 185.03 311.29 o 11 23 0 3000.53 2854.58 457.37 o 0 24 0 10023.71 11367.60 898.17 o 1 24 0 5080.25 5772.49 398.02 o 2 24 0 542.97 430.54 198.61 o 3 24 0 140.40 286.76 140.81 o 4 24 0 7234.72 7587.53 664.57 o 5 24 0 582.36 475.36 171.90 o 6 24 0 8061.07 6899.75 462.94 o 7 24 0 13037.97 12670.03 678.88 o 8 24 0 40.06 -136.68 198.38 o 9 24 0 14.36 -29.93 293.05 o 10 24 0 0.09 273.08 323.17 o 11 24 0 1.35 264.31 349.45 o 1 25 0 19438.03 18466.06 783.44 o 2 25 0 7196.16 7042.82 437.62 o 3 25 0 983.56 677.24 270.97 o 4 25 0 10367.39 11174.44 633.91 o 5 25 0 1602.44 2136.01 244.29 o 6 25 0 897.11 750.90 233.69 o 7 25 0 14132.56 14586.50 754.94 o 8 25 0 360.42 321.01 234.56 o 9 25 0 2529.39 1673.49 594.30 o 10 25 0 10854.90 12284.24 836.12 o 0 26 0 16932.35 16696.97 1208.85 o 1 26 0 192.71 306.64 170.39 o 2 26 0 0.76 256.73 164.90 o 3 26 0 58.50 -30.54 168.41 o 4 26 0 158.42 283.83 181.33 o 5 26 0 2835.19 3166.85 328.81 o 6 26 0 4619.33 5310.33 541.65 o 7 26 0 2266.71 2199.38 334.21 o 8 26 0 6253.83 7415.10 531.63 o 9 26 0 1533.96 1707.27 326.41 o 10 26 0 3352.81 3195.80 457.46 o 1 27 0 9.54 197.03 164.25 o 2 27 0 5086.99 5789.47 417.56 o 3 27 0 3659.60 3383.28 592.40 o 4 27 0 654.21 506.57 204.95 o 5 27 0 6391.68 6535.70 465.35 o 6 27 0 4221.01 3638.44 468.76 o 7 27 0 356.93 914.52 352.16 o 8 27 0 4038.25 6582.79 611.31 o 9 27 0 981.17 819.72 291.39 o 10 27 0 1933.62 1003.51 374.51 o 0 28 0 7086.70 6898.55 770.33 o 1 28 0 3658.50 3406.57 402.52 o 2 28 0 6390.99 6853.96 466.71 o 3 28 0 2417.55 2203.84 289.83 o 4 28 0 5266.94 5724.07 444.99 o 5 28 0 190.19 322.26 344.79 o 6 28 0 660.08 298.35 316.75 o 7 28 0 13122.56 14673.04 1416.73 o 8 28 0 5913.45 5753.75 586.52 o 9 28 0 1665.33 1348.56 372.60 o 1 29 0 376.98 389.77 272.57 o 2 29 0 4020.15 4948.94 560.30 o 3 29 0 4178.01 4965.51 420.95 o 4 29 0 916.07 1515.48 261.89 o 5 29 0 112.72 223.65 414.12 o 6 29 0 5.18 -294.23 294.23 o 7 29 0 358.17 728.82 378.19 o 8 29 0 2200.16 1750.88 427.13 o 9 29 0 3837.29 3806.58 501.73 o 0 30 0 29973.03 31950.49 2069.39 o 1 30 0 5.85 376.91 274.06 o 2 30 0 594.33 116.05 287.91 o 3 30 0 238.65 70.33 247.50 o 4 30 0 130.52 129.69 196.68 o 5 30 0 8101.44 8849.78 726.92 o 6 30 0 7565.37 8928.94 715.18 o 7 30 0 732.56 161.09 503.68 o 8 30 0 1091.94 1181.31 423.65 o 1 31 0 7539.44 7404.02 753.41 o 2 31 0 352.34 782.77 350.15 o 3 31 0 1652.03 1410.65 374.06 o 4 31 0 2185.83 2278.47 308.36 o 5 31 0 93.59 197.36 249.10 o 6 31 0 84.73 -219.98 319.21 o 7 31 0 184.15 406.41 392.77 o 8 31 0 29.77 -114.45 351.80 o 0 32 0 2941.90 2227.77 567.01 o 1 32 0 1038.78 1174.95 356.41 o 2 32 0 2483.06 2695.35 421.83 o 3 32 0 402.14 454.88 301.05 o 4 32 0 2985.73 3018.23 629.02 o 5 32 0 4.02 -256.57 256.57 o 6 32 0 106.15 118.75 378.58 o 7 32 0 4681.05 5210.72 1036.66 o 1 33 0 1065.72 760.33 364.62 o 2 33 0 7523.50 7099.56 619.35 o 3 33 0 3981.27 4727.11 879.28 o 4 33 0 264.44 830.37 337.40 o 5 33 0 390.85 413.73 300.70 o 6 33 0 172.69 474.27 331.55 o 7 33 0 1233.08 640.79 616.83 o 0 34 0 366.12 315.74 517.11 o 1 34 0 2856.84 3526.27 507.95 o 2 34 0 49.44 200.12 335.63 o 3 34 0 17.63 -35.87 311.03 o 4 34 0 216.04 671.51 521.23 o 5 34 0 1290.53 1365.33 499.27 o 6 34 0 949.36 419.94 375.80 o 1 35 0 5526.84 5426.28 587.88 o 2 35 0 1350.86 1194.57 414.29 o 3 35 0 1288.30 765.56 367.31 o 4 35 0 6008.91 7481.22 678.88 o 5 35 0 928.55 -154.16 459.26 o 0 36 0 1002.07 1173.83 597.45 o 1 36 0 52.78 104.90 345.92 o 2 36 0 38.20 -136.63 375.45 o 3 36 0 624.27 69.43 359.91 o 4 36 0 1009.48 1954.54 488.23 o 1 37 0 6401.06 6700.69 874.24 o 2 37 0 288.69 158.14 368.28 o 3 37 0 4678.79 5300.74 819.73 o 0 38 0 2072.53 1345.63 681.34 o 1 38 0 181.51 77.51 395.51 o -14 1 1 5213.89 5587.24 506.78 o -13 1 1 653.87 709.98 224.22 o -12 1 1 4316.41 4507.73 328.47 o -11 1 1 497.74 440.96 186.36 o -10 1 1 22034.66 22482.28 848.24 o -9 1 1 141.35 178.61 140.24 o -8 1 1 50655.73 49595.44 1762.05 o -7 1 1 1468.60 1409.91 156.69 o -6 1 1 73449.88 70039.80 2006.41 o -5 1 1 201.29 96.05 89.87 o -4 1 1 40065.55 41501.36 1191.21 o -3 1 1 316.44 292.63 54.80 o -2 1 1 6.71 -34.67 34.67 o -1 1 1 115859.66 116917.39 4276.21 o 1 1 1 59538.61 56282.13 2084.14 o 2 1 1 11987.73 12534.59 375.54 o 3 1 1 18055.22 18322.67 544.00 o 4 1 1 615.95 429.44 66.96 o 5 1 1 6433.96 6140.35 240.85 o 6 1 1 62.99 -31.40 60.75 o 7 1 1 2710.11 2617.08 205.07 o 8 1 1 1726.56 1740.32 187.01 o 9 1 1 134.09 469.12 174.77 o 10 1 1 1303.56 1140.64 209.10 o 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