Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 3 (March 2013)

organic compounds

Acta Cryst. (2013). E69, o375    [ doi:10.1107/S1600536813003292 ]

3,3'-(1-Oxopropane-1,3-di­yl)bis­(1,3-thia­zolidine-2-thione) chloro­benzene hemisolvate

C. Franzel, A. Purdy and R. J. Butcher

Abstract: The title compound, C9H12N2OS4·0.5C6H5Cl, which contains two 1,3-thia­zolidine-2-thione rings, is a by-product of the synthesis of 3-acryloyl-1,3-thia­zolidine-2-thione. The dihedral angle between these rings is 79.95 (9)°, with both rings displaying a twisted conformation. The twist angle of the amide group is 5.6 (1)°. In the crystal, the molecules are linked into [001] chains by C-H...O interactions. The chloro­benzene solvent mol­ecule was found to show unresolvable disorder about a centre of inversion and its contribution to the scattering was removed with the SQUEEZE option in PLATON [Spek (2009). Acta Cryst. D65, 148-155].

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