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[Contents scheme]

Acta Cryst. (2013). E69, m143
[ doi:10.1107/S1600536813003462 ]

Tris[dimethyl (benzoylamido)phosphato-[kappa]2O,O'](1,10-phenanthroline-[kappa]2N,N')neodymium(III)

N. S. Kariaka, V. A. Trush, V. V. Medviediev, T. Y. Sliva and V. M. Amirkhanov


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B Crystal system given = triclinic PLAT230_ALERT_2_B Hirshfeld Test Diff for O8 -- C18 .. 10.5 su PLAT230_ALERT_2_B Hirshfeld Test Diff for O24 -- C66 .. 11.0 su PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 26
Alert level C PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.6 Ratio PLAT220_ALERT_2_C Large Non-Solvent C Ueq(max)/Ueq(min) ... 3.4 Ratio PLAT230_ALERT_2_C Hirshfeld Test Diff for C22 -- C23 .. 5.3 su PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O2 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O5 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O6 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C24 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O22 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for O8 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Nd2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for P6 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 4.825 PLAT973_ALERT_2_C Large Calcd. Positive Residual Density on Nd2 1.14 eA-3
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT112_ALERT_2_G ADDSYM Detects Additional (Pseudo) Symm. Elem... B PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00300 Deg. PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Nd2 -- O13 .. 5.3 su PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 14 ALERT level C = Check. Ensure it is not caused by an omission or oversight 7 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 17 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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