[Open access]

Acta Cryst. (2013). E69, i18
[ doi:10.1107/S1600536813003875 ]

The Mg member of the isotypic series MTe6O13

M. Shirkhanlou and M. Weil


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for Te1 -- O1 .. 8.8 su PLAT230_ALERT_2_B Hirshfeld Test Diff for Te1 -- O2_k .. 10.8 su PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.376 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -1.54 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 1.10A from O2 . 1.13 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 1.10A from O5 . 0.92 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 1.04A from O5 . 0.92 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.99A from O2 . 0.90 eA-3 PLAT975_ALERT_2_C Positive Residual Density at 0.97A from O5 . 0.85 eA-3
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 7.60 PLAT152_ALERT_1_G The Supplied and Calc. Volume s.1. Differ by ... 3 Units PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 16
0 ALERT level A = Most likely a serious problem - resolve or explain 3 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 9 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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