# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' DMMXI017a_abs in P21/c 14' _shelx_refln_list_code 4 _shelx_F_calc_maximum 336.86 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.6619 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 8.8437 _cell_length_b 8.8390 _cell_length_c 17.2662 _cell_angle_alpha 90.000 _cell_angle_beta 103.674 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11733.55 12563.72 215.67 o 3 0 0 113472.15 115362.36 1817.27 o 4 0 0 63512.57 65860.74 833.33 o 5 0 0 760.46 844.25 46.28 o 6 0 0 29081.08 30542.19 455.13 o 7 0 0 39097.15 39524.07 799.06 o 8 0 0 12387.26 12849.51 316.92 o 9 0 0 2968.54 2828.15 197.94 o 10 0 0 21644.65 21682.63 1025.00 o 11 0 0 10310.76 10225.33 456.00 o 12 0 0 39.21 5.95 64.01 o 2 1 0 57542.33 58989.54 604.44 o 3 1 0 8401.57 8379.49 149.99 o 4 1 0 12593.79 12693.38 166.58 o 5 1 0 32063.44 31678.69 389.82 o 6 1 0 6998.94 7213.84 120.27 o 7 1 0 649.92 691.25 47.79 o 8 1 0 12127.45 12964.32 251.61 o 9 1 0 13385.42 13450.85 283.46 o 10 1 0 7.34 28.06 55.58 o 11 1 0 4908.09 4855.19 216.17 o 12 1 0 5272.75 5477.73 279.51 o 0 2 0 13194.73 13848.02 182.35 o 1 2 0 8619.55 8986.00 122.48 o 2 2 0 163.25 203.73 19.29 o 3 2 0 6075.01 6123.39 102.10 o 4 2 0 10860.18 11042.88 147.37 o 5 2 0 1267.74 1267.08 45.88 o 6 2 0 3381.89 3448.38 91.08 o 7 2 0 2929.46 2891.15 88.18 o 8 2 0 2511.94 2554.11 111.70 o 9 2 0 717.05 687.10 75.01 o 10 2 0 1404.59 1418.94 91.20 o 11 2 0 659.91 487.67 58.87 o 12 2 0 12.28 89.02 72.52 o 1 3 0 175.80 228.22 13.09 o 2 3 0 60.90 71.08 14.64 o 3 3 0 946.07 998.34 41.54 o 4 3 0 1028.28 1041.13 40.71 o 5 3 0 93.69 95.24 25.12 o 6 3 0 731.26 829.71 47.14 o 7 3 0 1244.17 1130.60 63.48 o 8 3 0 1222.85 1159.75 80.06 o 9 3 0 108.72 139.71 39.45 o 10 3 0 295.57 284.21 49.24 o 11 3 0 1801.06 1844.89 123.41 o 12 3 0 285.27 266.80 61.77 o 0 4 0 34996.58 34852.02 489.25 o 1 4 0 19091.23 18960.72 212.62 o 2 4 0 7686.59 7836.11 108.54 o 3 4 0 17258.63 17016.86 334.28 o 4 4 0 16309.51 15947.81 247.21 o 5 4 0 62.32 94.02 21.12 o 6 4 0 13727.69 14385.15 278.70 o 7 4 0 18126.96 18403.23 281.72 o 8 4 0 2863.21 2763.55 122.31 o 9 4 0 2626.87 2431.04 141.75 o 10 4 0 11986.87 12691.42 335.46 o 11 4 0 5282.01 5266.73 211.60 o 12 4 0 158.40 65.96 73.42 o 1 5 0 24481.69 24110.22 282.68 o 2 5 0 29808.68 29525.70 343.98 o 3 5 0 793.31 785.32 58.39 o 4 5 0 11377.36 11099.42 200.31 o 5 5 0 18769.70 18700.24 277.26 o 6 5 0 5000.55 5014.49 120.18 o 7 5 0 2612.43 2507.08 109.96 o 8 5 0 14795.67 14713.42 396.45 o 9 5 0 11958.33 11964.51 335.09 o 10 5 0 59.35 61.43 42.00 o 11 5 0 7845.05 8288.99 278.54 o 0 6 0 26613.96 26187.96 373.40 o 1 6 0 6102.97 6097.99 94.19 o 2 6 0 2159.07 2120.27 55.33 o 3 6 0 20956.69 20655.20 547.54 o 4 6 0 5873.20 5849.41 158.58 o 5 6 0 430.95 398.64 36.95 o 6 6 0 8577.23 8765.42 187.65 o 7 6 0 11996.36 11992.72 267.36 o 8 6 0 456.18 409.37 59.23 o 9 6 0 2821.37 2710.15 145.74 o 10 6 0 9168.75 9908.71 306.74 o 11 6 0 3028.77 3139.59 400.30 o 1 7 0 4617.34 4502.26 105.06 o 2 7 0 8743.34 8480.82 193.36 o 3 7 0 688.17 690.39 64.92 o 4 7 0 1875.35 1809.73 105.95 o 5 7 0 5716.85 6016.45 145.27 o 6 7 0 3722.54 3888.30 119.43 o 7 7 0 322.60 319.69 46.31 o 8 7 0 4632.20 4735.69 189.90 o 9 7 0 1761.36 1720.69 137.16 o 10 7 0 365.20 277.20 69.01 o 0 8 0 10003.66 9798.99 292.19 o 1 8 0 759.11 786.33 50.34 o 2 8 0 450.24 428.95 48.83 o 3 8 0 1592.45 1511.63 100.80 o 4 8 0 2290.92 1964.96 118.66 o 5 8 0 20.03 38.51 28.02 o 6 8 0 379.38 283.28 46.72 o 7 8 0 1015.03 1101.10 104.97 o 8 8 0 870.85 1003.06 148.15 o 9 8 0 23.35 30.12 51.60 o 1 9 0 10772.87 10221.87 229.28 o 2 9 0 10440.00 10220.27 257.67 o 3 9 0 1254.71 1396.46 136.72 o 4 9 0 3067.29 2973.25 154.95 o 5 9 0 9267.96 9188.45 292.96 o 6 9 0 1661.50 1536.55 116.77 o 7 9 0 238.08 180.99 71.98 o 8 9 0 5654.71 5891.27 308.72 o 0 10 0 15182.37 15114.88 437.29 o 1 10 0 6544.37 6513.32 206.75 o 2 10 0 1940.06 1943.65 111.23 o 3 10 0 10059.47 10040.74 273.82 o 4 10 0 7719.88 7841.46 275.75 o 5 10 0 87.49 119.68 51.26 o 6 10 0 6427.77 6550.36 315.77 o 7 10 0 7636.48 7747.50 306.80 o 1 11 0 10603.04 10784.63 294.60 o 2 11 0 13017.42 13164.20 427.62 o 3 11 0 1585.90 1520.25 106.36 o 4 11 0 2940.89 3086.47 156.51 o 5 11 0 9616.63 9808.77 302.66 o 6 11 0 4601.40 4728.10 280.62 o 7 11 0 168.44 180.39 132.34 o 0 12 0 737.04 752.75 137.12 o 1 12 0 309.02 263.06 64.40 o 2 12 0 54.54 83.61 42.11 o 3 12 0 839.46 882.84 95.16 o 4 12 0 725.51 672.17 82.41 o 5 12 0 53.27 120.20 86.17 o 2 13 0 873.47 886.32 196.94 o -12 1 1 136.89 89.62 50.33 o -11 1 1 4077.21 4213.81 198.05 o -10 1 1 9185.75 9561.75 239.94 o -9 1 1 333.98 372.16 47.75 o -8 1 1 2922.47 3037.37 105.97 o -7 1 1 18264.19 18795.50 337.66 o -6 1 1 8819.12 9093.00 154.92 o -5 1 1 3697.95 3739.71 87.72 o -4 1 1 40149.71 39850.38 515.51 o -3 1 1 27142.14 27756.94 278.96 o -2 1 1 337.18 356.09 13.85 o 1 1 1 6587.59 6703.73 102.89 o 2 1 1 5589.48 5907.86 121.53 o 3 1 1 28588.82 28955.99 557.18 o 4 1 1 16766.61 17439.19 230.12 o 5 1 1 71.99 66.52 16.59 o 6 1 1 11030.28 11560.71 177.03 o 7 1 1 11110.34 11440.64 215.38 o 8 1 1 1529.01 1547.81 76.13 o 9 1 1 3098.34 2919.66 121.68 o 10 1 1 4899.73 4957.39 167.03 o 11 1 1 1369.13 1357.09 101.56 o 12 1 1 102.96 108.38 48.28 o -12 2 1 7359.50 7714.22 393.35 o -11 2 1 4792.15 5044.45 196.25 o -10 2 1 315.20 238.79 43.50 o -9 2 1 10332.49 10745.59 253.54 o -8 2 1 13309.19 13586.97 280.81 o -7 2 1 634.29 629.12 47.30 o -6 2 1 13164.43 13299.37 191.99 o -5 2 1 31947.71 32138.97 401.65 o -4 2 1 4936.86 4893.01 94.39 o -3 2 1 9296.09 9263.29 135.97 o -2 2 1 62943.37 62549.16 689.28 o -1 2 1 27152.70 27310.00 316.96 o 0 2 1 4034.87 4197.68 67.42 o 1 2 1 32308.32 32892.87 519.41 o 2 2 1 15387.55 15266.32 173.86 o 3 2 1 353.29 378.51 18.38 o 4 2 1 22178.73 22536.53 418.91 o 5 2 1 33924.24 34607.88 692.85 o 6 2 1 2040.51 2137.81 72.28 o 7 2 1 4988.90 5073.04 134.17 o 8 2 1 14745.54 14956.22 301.46 o 9 2 1 5549.78 5664.31 177.28 o 10 2 1 888.56 948.38 81.05 o 11 2 1 9760.84 9863.79 287.38 o 12 2 1 6145.86 6089.67 256.51 o -12 3 1 223.43 55.94 47.00 o -11 3 1 11258.62 11461.82 441.39 o -10 3 1 13052.98 13502.37 338.12 o -9 3 1 1523.04 1476.88 91.66 o -8 3 1 8241.32 8160.60 214.67 o -7 3 1 24999.23 25322.71 486.41 o -6 3 1 16179.56 16155.92 287.84 o -5 3 1 2388.92 2430.93 71.05 o -4 3 1 59705.79 59955.92 836.60 o -3 3 1 45094.98 43989.66 587.68 o -2 3 1 8301.95 8427.42 136.33 o -1 3 1 41828.81 40315.73 478.42 o 0 3 1 71869.08 70574.07 660.99 o 1 3 1 27442.75 28049.50 300.49 o 2 3 1 13917.46 14120.86 198.85 o 3 3 1 52357.81 51567.58 556.53 o 4 3 1 30432.23 30190.19 388.04 o 5 3 1 328.01 333.64 31.48 o 6 3 1 19578.16 19768.04 388.34 o 7 3 1 26581.64 26217.64 629.08 o 8 3 1 2308.93 2296.41 110.70 o 9 3 1 4352.14 4685.03 165.91 o 10 3 1 15079.92 16000.68 343.55 o 11 3 1 3510.37 3493.41 166.83 o 12 3 1 743.82 572.58 194.93 o -12 4 1 3871.62 3965.21 243.01 o -11 4 1 1346.19 1423.20 112.12 o -10 4 1 1090.33 1125.03 93.15 o -9 4 1 6581.42 6670.01 222.84 o -8 4 1 7090.26 7133.15 184.38 o -7 4 1 2.15 33.78 24.19 o -6 4 1 9210.91 9001.32 178.71 o -5 4 1 19390.47 18795.73 291.64 o -4 4 1 3386.97 3378.12 86.49 o -3 4 1 5735.91 5651.45 128.80 o -2 4 1 26165.30 25690.38 326.36 o -1 4 1 18219.22 17634.86 273.78 o 0 4 1 32.70 56.30 9.34 o 1 4 1 12503.81 12206.79 162.23 o 2 4 1 24524.57 24139.29 341.05 o 3 4 1 2480.72 2501.61 74.15 o 4 4 1 5872.62 5646.19 123.80 o 5 4 1 15896.21 15753.29 256.25 o 6 4 1 6116.08 6263.79 137.26 o 7 4 1 656.89 718.37 48.89 o 8 4 1 6836.37 6966.48 217.25 o 9 4 1 4676.49 4679.89 173.62 o 10 4 1 25.66 14.30 47.12 o 11 4 1 2712.92 2916.09 157.28 o 12 4 1 3233.45 3909.04 404.66 o -11 5 1 185.23 134.52 45.30 o -10 5 1 17.86 -40.02 46.39 o -9 5 1 5.90 -31.82 46.96 o -8 5 1 164.28 126.84 39.96 o -7 5 1 389.84 328.77 35.45 o -6 5 1 161.80 106.95 23.96 o -5 5 1 88.49 142.05 24.25 o -4 5 1 140.41 197.05 26.69 o -3 5 1 52.05 58.20 13.38 o -2 5 1 14.35 18.50 19.08 o -1 5 1 161.00 229.52 15.35 o 0 5 1 538.14 629.22 27.54 o 1 5 1 117.45 130.24 14.88 o 2 5 1 319.91 353.09 21.35 o 3 5 1 549.96 603.06 32.51 o 4 5 1 40.09 8.74 16.76 o 5 5 1 66.05 90.66 30.83 o 6 5 1 67.92 113.42 25.99 o 7 5 1 60.17 51.31 30.03 o 8 5 1 192.98 186.06 69.49 o 9 5 1 10.57 -12.06 57.60 o 10 5 1 55.25 -15.87 46.25 o 11 5 1 78.73 118.18 57.78 o -11 6 1 1465.20 1487.74 204.84 o -10 6 1 162.00 105.36 47.66 o -9 6 1 1295.45 1264.40 99.12 o -8 6 1 1968.77 2046.78 119.83 o -7 6 1 679.16 612.05 49.67 o -6 6 1 1232.27 1188.19 61.95 o -5 6 1 2841.22 2820.66 92.22 o -4 6 1 464.64 468.17 49.94 o -3 6 1 1682.29 1786.63 72.12 o -2 6 1 3040.14 2938.37 99.12 o -1 6 1 1789.59 1756.46 43.13 o 0 6 1 2883.90 2904.74 59.59 o 1 6 1 3379.11 3408.17 69.37 o 2 6 1 1183.97 1094.16 57.80 o 3 6 1 276.36 300.62 26.80 o 4 6 1 7658.01 7497.86 184.04 o 5 6 1 6790.63 6984.00 177.62 o 6 6 1 30.46 43.98 21.76 o 7 6 1 4169.20 4302.80 169.53 o 8 6 1 4184.16 3895.54 247.01 o 9 6 1 1366.09 1442.78 109.21 o 10 6 1 1457.22 1506.12 117.60 o 11 6 1 3587.94 3868.67 414.06 o -11 7 1 4495.63 4430.98 436.89 o -10 7 1 9811.64 9593.54 342.25 o -9 7 1 1623.06 1647.89 115.50 o -8 7 1 2271.82 2126.05 153.48 o -7 7 1 13839.09 14380.13 275.64 o -6 7 1 8485.12 8704.09 188.42 o -5 7 1 2589.62 2667.08 103.62 o -4 7 1 21623.14 20710.90 430.73 o -3 7 1 17384.28 16842.81 362.02 o -2 7 1 122.70 104.61 20.73 o -1 7 1 13495.33 13130.29 193.10 o 0 7 1 26575.45 26262.21 316.18 o 1 7 1 1374.20 1352.11 64.39 o 2 7 1 7805.28 7283.82 213.86 o 3 7 1 28301.09 28089.80 525.75 o 4 7 1 9007.49 8983.06 255.30 o 5 7 1 1786.59 1781.00 80.34 o 6 7 1 21308.73 21652.23 372.93 o 7 7 1 11684.17 12079.34 310.37 o 8 7 1 448.39 348.36 77.82 o 9 7 1 8404.29 8205.63 307.02 o 10 7 1 8851.99 9495.64 345.11 o -9 8 1 10557.32 10120.88 629.22 o -8 8 1 8982.27 9497.91 831.61 o -7 8 1 154.19 218.42 54.69 o -6 8 1 11234.00 11313.34 276.55 o -5 8 1 20116.29 20185.67 391.46 o -4 8 1 2654.80 2498.77 132.88 o -3 8 1 9131.87 8973.43 257.11 o -2 8 1 30242.18 28803.65 482.93 o -1 8 1 9665.02 9260.26 186.49 o 0 8 1 2316.22 2235.97 93.94 o 1 8 1 28472.75 27142.63 458.87 o 2 8 1 16768.07 16697.91 334.06 o 3 8 1 57.75 33.16 32.47 o 4 8 1 17671.08 17317.46 484.31 o 5 8 1 22661.04 22551.71 489.00 o 6 8 1 2530.03 2643.95 131.27 o 7 8 1 3573.54 3500.81 182.88 o 8 8 1 14628.83 15083.70 429.46 o 9 8 1 5911.72 6002.09 266.94 o 10 8 1 112.24 35.55 83.11 o -8 9 1 648.17 659.88 109.41 o -7 9 1 2367.91 2356.84 243.69 o -6 9 1 1630.36 1690.21 123.58 o -5 9 1 156.05 81.99 32.34 o -4 9 1 2839.46 2825.32 150.74 o -3 9 1 3404.10 3154.05 153.15 o -2 9 1 27.67 85.65 34.72 o -1 9 1 4762.58 4461.98 142.38 o 0 9 1 4135.03 4005.66 134.60 o 1 9 1 46.80 46.98 32.34 o 2 9 1 4247.66 4029.14 172.00 o 3 9 1 7049.64 6979.22 239.81 o 4 9 1 581.57 535.05 69.03 o 5 9 1 1959.82 1909.57 128.05 o 6 9 1 7004.84 7450.31 327.71 o 7 9 1 2497.66 2916.12 206.45 o 8 9 1 184.47 79.05 74.27 o -7 10 1 30.70 -1.30 50.32 o -6 10 1 260.06 269.30 62.70 o -5 10 1 125.25 165.27 46.79 o -4 10 1 4.94 -26.03 38.22 o -3 10 1 460.10 298.66 58.85 o -2 10 1 55.42 39.78 39.06 o -1 10 1 41.95 6.18 45.31 o 0 10 1 140.22 175.14 40.07 o 1 10 1 351.32 341.68 68.42 o 2 10 1 790.31 857.56 88.06 o 3 10 1 31.56 31.78 43.35 o 4 10 1 409.40 514.59 72.16 o 5 10 1 531.68 579.15 79.32 o 6 10 1 470.22 383.06 93.33 o 7 10 1 295.94 337.97 82.93 o -7 11 1 2321.02 2261.35 337.51 o -6 11 1 1506.54 1442.86 127.56 o -5 11 1 214.83 243.55 55.53 o -4 11 1 4532.98 4363.63 186.98 o -3 11 1 3592.11 3715.77 167.69 o -2 11 1 317.22 232.31 55.92 o -1 11 1 2528.27 2583.77 149.95 o 0 11 1 4043.66 4195.12 158.42 o 1 11 1 1245.21 1354.54 111.34 o 2 11 1 637.21 692.22 72.20 o 3 11 1 2922.22 2775.08 144.38 o 4 11 1 1723.03 1567.51 112.57 o 5 11 1 23.01 -16.57 50.66 o 6 11 1 1114.95 1270.38 149.01 o 7 11 1 1507.95 1552.70 285.23 o -5 12 1 11305.35 11030.83 521.94 o -4 12 1 1915.25 1872.64 143.81 o -3 12 1 4581.39 4638.30 220.57 o -2 12 1 13627.26 14155.25 472.20 o -1 12 1 7774.79 8027.47 264.67 o 0 12 1 142.51 69.22 61.75 o 1 12 1 7965.50 7917.95 292.85 o 2 12 1 11804.91 12413.70 350.09 o 3 12 1 840.08 792.40 83.90 o 4 12 1 4142.38 4028.01 204.35 o 5 12 1 9645.90 10236.92 782.43 o -2 13 1 62.73 -9.36 77.63 o 1 13 1 1738.22 1754.58 267.62 o 2 13 1 1498.84 1125.03 220.29 o -12 0 2 1646.07 1835.77 283.72 o -11 0 2 19642.62 21095.24 842.39 o -10 0 2 21250.94 21582.85 685.52 o -9 0 2 97.91 80.83 45.61 o -8 0 2 25906.10 27749.55 864.15 o -7 0 2 46359.59 48145.43 1001.77 o -6 0 2 21451.91 22573.34 499.07 o -5 0 2 12805.71 12593.81 342.62 o -4 0 2 90606.90 86045.66 1186.89 o -3 0 2 89939.39 90974.74 1093.77 o -2 0 2 169.09 256.41 17.20 o 1 0 2 831.54 1058.87 81.36 o 2 0 2 15423.46 16794.84 441.00 o 3 0 2 72659.62 74310.74 1220.01 o 4 0 2 17980.69 17866.82 332.73 o 5 0 2 575.03 665.64 46.80 o 6 0 2 20272.53 20308.58 343.06 o 7 0 2 14523.54 15193.35 429.02 o 8 0 2 2154.66 2262.50 120.94 o 9 0 2 15626.56 14908.86 430.21 o 10 0 2 12381.60 12183.28 492.81 o 11 0 2 1446.96 1503.69 170.94 o 12 0 2 2231.26 2197.93 239.47 o -12 1 2 8063.77 8383.29 349.82 o -11 1 2 1897.84 1904.52 192.51 o -10 1 2 2601.93 2801.09 167.77 o -9 1 2 15841.36 16411.65 420.13 o -8 1 2 7074.30 7233.35 170.38 o -7 1 2 24.56 45.10 26.63 o -6 1 2 23542.54 23814.54 437.87 o -5 1 2 34012.98 34331.31 363.28 o -4 1 2 3044.38 3028.65 62.89 o -3 1 2 9831.62 9725.95 122.82 o -2 1 2 37156.89 37984.04 425.32 o -1 1 2 21383.60 21900.96 216.09 o 1 1 2 34840.17 35741.44 647.49 o 2 1 2 9771.78 9491.27 128.98 o 3 1 2 4.85 36.35 15.73 o 4 1 2 12539.19 13158.12 177.31 o 5 1 2 12791.67 12847.02 193.12 o 6 1 2 241.38 252.64 25.94 o 7 1 2 5220.46 5330.12 116.55 o 8 1 2 12883.94 12850.44 268.20 o 9 1 2 1385.52 1441.79 85.18 o 10 1 2 3972.95 4063.58 168.63 o 11 1 2 6984.89 6913.81 233.06 o 12 1 2 2904.91 2596.82 165.06 o -13 2 2 298.57 274.36 112.27 o -12 2 2 27.71 -60.87 69.64 o -11 2 2 1813.71 1880.18 171.55 o -10 2 2 2133.02 2066.53 108.74 o -9 2 2 242.32 210.17 41.43 o -8 2 2 2978.97 3062.48 120.75 o -7 2 2 5032.22 5168.37 151.41 o -6 2 2 4127.06 4143.31 100.57 o -5 2 2 1309.25 1382.15 51.39 o -4 2 2 7523.26 7654.59 122.80 o -3 2 2 10016.70 10056.35 113.34 o -2 2 2 79.58 113.82 13.97 o -1 2 2 449.72 476.88 21.99 o 0 2 2 18016.36 18448.94 221.86 o 1 2 2 83.54 72.55 12.40 o 2 2 2 487.94 616.58 25.78 o 3 2 2 4997.65 5106.73 78.82 o 4 2 2 2300.32 2589.63 83.19 o 5 2 2 443.65 512.71 41.08 o 6 2 2 1138.18 1096.69 53.75 o 7 2 2 1177.34 1111.80 62.27 o 8 2 2 271.94 290.44 40.98 o 9 2 2 1747.33 1696.31 96.63 o 10 2 2 491.82 456.59 55.36 o 11 2 2 26.36 58.03 55.20 o 12 2 2 692.60 783.51 107.28 o -12 3 2 292.71 329.05 61.17 o -11 3 2 231.56 212.56 50.02 o -10 3 2 8.12 -17.67 46.66 o -9 3 2 103.26 75.08 38.60 o -8 3 2 94.23 111.49 34.45 o -7 3 2 2.76 20.21 22.28 o -6 3 2 299.55 274.59 27.92 o -5 3 2 44.03 59.54 15.94 o -4 3 2 512.67 457.70 26.49 o -3 3 2 97.08 98.83 15.21 o -2 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2706.73 2644.04 102.79 o 6 4 2 17806.36 18184.16 312.20 o 7 4 2 21870.85 22035.40 596.73 o 8 4 2 61.33 28.71 35.10 o 9 4 2 8365.24 8040.30 233.35 o 10 4 2 13973.68 15157.87 344.51 o 11 4 2 1122.71 1114.43 99.21 o 12 4 2 1257.30 1081.60 212.38 o -11 5 2 2276.41 2455.54 147.47 o -10 5 2 2522.22 2518.54 143.54 o -9 5 2 8551.47 8646.42 344.84 o -8 5 2 7714.92 7821.14 208.29 o -7 5 2 358.27 404.02 44.03 o -6 5 2 16923.05 17196.11 283.79 o -5 5 2 19801.03 19146.07 305.49 o -4 5 2 1773.45 1798.45 63.77 o -3 5 2 16601.83 15907.24 277.32 o -2 5 2 41193.00 40864.92 561.58 o -1 5 2 7215.50 7029.34 122.66 o 0 5 2 19849.06 19507.82 223.21 o 1 5 2 52046.27 50994.57 592.22 o 2 5 2 18672.06 18538.82 390.64 o 3 5 2 2314.68 2339.01 66.83 o 4 5 2 26559.19 26243.99 341.63 o 5 5 2 26223.94 26574.57 489.98 o 6 5 2 2030.01 2072.26 88.95 o 7 5 2 11852.03 11692.54 292.31 o 8 5 2 22980.38 22894.69 476.97 o 9 5 2 5649.66 5579.59 300.73 o 10 5 2 2462.31 2550.82 147.21 o 11 5 2 13186.41 13716.04 370.19 o -11 6 2 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