[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o351
[ doi:10.1107/S1600536813003231 ]

(E)-Ethyl 2-anilino-5-[3-(dimethylamino)acryloyl]-4-phenylthiophene-3-carboxylate

Y. N. Mabkhot, A. Barakat, F. Alatibi, M. I. Choudhary and S. Yousuf


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT031_ALERT_4_B Refined Extinction Parameter within Range ...... 2.000 Sigma PLAT919_ALERT_3_B Reflection # Likely Affected by the Beamstop ... 1 PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1 PLAT939_ALERT_3_B Large Value of Not (SHELXL) Weight Optimized S . 113.56
Alert level C PLAT360_ALERT_2_C Short C(sp3)-C(sp3) Bond C23 - C24 ... 1.43 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.078 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00300 Deg. PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 273 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 273 K PLAT380_ALERT_4_G Check Incorrectly? Oriented X(sp2)-Methyl Moiety C20
0 ALERT level A = Most likely a serious problem - resolve or explain 4 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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