[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m142
[ doi:10.1107/S1600536813003632 ]

Tris(3,4,7,8-tetramethyl-1,10-phenanthrolin-1-ium) hexacyanidocobaltate(III) pentahydrate

A.-Y. Hu, D.-Y. Yu and A.-H. Yuan


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT417_ALERT_2_C Short Inter D-H..H-D H1A .. H5A .. 2.11 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.455 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 80
Alert level G PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 4 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 13 PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00200 Deg. PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 20 Perc. PLAT794_ALERT_5_G Note: Tentative Bond Valency for Co1 (III) 2.59 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 2 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 7 PLAT961_ALERT_5_G Dataset Contains no Negative Intensities ....... !
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 9 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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