Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 3 (March 2013)

organic compounds

Acta Cryst. (2013). E69, o376    [ doi:10.1107/S1600536813003206 ]


B.-H. Qu, X.-C. Jia, J. Li and M.-Y. He

Abstract: In the title compound, C10H6F2N4, the Car-N bonds are slightly shortened with respect to a standard aniline C-N bond [1.3580 (16) and 1.3618 (16) versus 1.39 Å], thus indicating some [pi]-[pi] conjgation with the electron-acceptor CN groups. The mol­ecule, except for two C atom of the ethyl­ene bridge, is nearly planar, the largest deviation of the other non-H atoms from the mean plane being 0.309 (2) Å. The N-C-C-N torsion angle involving the ethyl­ene bridge is 50.23 (18)°. In the crystal, mol­ecules are connected by pairs of N-H...N hydrogen bonds into chains along [21-1].

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