Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 3 (March 2013)

metal-organic compounds

Acta Cryst. (2013). E69, m167    [ doi:10.1107/S1600536813004674 ]

Bis[(E)-3-(4-meth­oxy­phen­yl)prop-2-enoato]triphenyl­anti­mony(V) benzene monosolvate

P. V. Andreev, N. V. Somov, O. S. Kalistratova, A. V. Gushchin and E. V. Chuprunov

Abstract: The asymmetric unit of the title compound, [Sb(C6H5)3(C10H9O3)2]·C6H6, contains one organometallic mol­ecule and one benzene mol­ecule that is disordered over two sets of sites with an occupancy ratio of 0.556 (15):0.444 (15). The SbV atom is in a distorted trigonal-bipyramidal environment with the carboxyl­ate O atoms in axial positions and phenyl C atoms in the equatorial plane. As a result of additional Sb...O inter­actions, one of the C-Sb-C angles is widened to 140.19 (6)°.

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