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[Contents scheme]

Acta Cryst. (2013). E69, m164
[ doi:10.1107/S1600536813004510 ]

Bis[2-(thiophen-2-yl)quinoxaline-[kappa]N4]silver(I) tetrafluoridoborate

G. Crundwell


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for C9 -- C10 .. 10.0 su PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW .gt. 10 Outliers . 1
Alert level C PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1 C24 H16 Ag N4 S2 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 14.289 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.146 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 10 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1 PLAT918_ALERT_3_C Reflection(s) # with I(obs) much smaller I(calc) 1
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 5 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained Atom Sites .... 5 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.14 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT244_ALERT_4_G Low 'Solvent' Ueq as Compared to Neighbors of B1 PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 55 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 229
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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