[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m255-m256
[ doi:10.1107/S1600536813009203 ]

catena-Poly[[(1,10-phenanthroline-[kappa]2N,N')copper(II)]-[mu]-2,2'-iminodibenzoato-[kappa]4O,O':O'',O''']

C. Yuste-Vivas, J. T. Coutinho, L. C. J. Pereira and M. R. Silva


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT707_ALERT_1_C D...A Calc 2.706(3), Rep 2.701(5), Dev.. 1.67 Sigma N1 -O3 1.555 1.555 # 62 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 4 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 4
Alert level G PLAT004_ALERT_5_G Info: Polymeric Structure Found with Dimension . 1 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 5.03 PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 1 O1 -CU1 -N2 -C15 142.70 0.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 6 O1 -CU1 -N2 -C26 -40.20 0.80 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 12 O4 -CU1 -N3 -C24 130.90 0.60 6.565 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 17 O4 -CU1 -N3 -C25 -48.80 0.70 6.565 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 23 N2 -CU1 -O1 -C1 -71.50 0.80 1.555 1.555 1.555 1.555 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Cu1 (II) 2.29 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 6
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 13 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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