[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o723
[ doi:10.1107/S1600536813009720 ]

1,5-Bis[1-(4-bromophenyl)ethylidene]thiocarbonohydrazide

Z. Gao


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT341_ALERT_3_B Low Bond Precision on C-C Bonds ............... 0.0152 Ang PLAT414_ALERT_2_B Short Intra D-H..H-X H3 .. H11A .. 1.82 Ang.
Alert level C CRYSC01_ALERT_1_C The word below has not been recognised as a standard identifier. block CRYSC01_ALERT_1_C No recognised colour has been given for crystal colour. PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 46 Perc. PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given ..... ? PLAT234_ALERT_4_C Large Hirshfeld Difference C31 -- C32 .. 0.17 Ang. PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C7 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C32 PLAT250_ALERT_2_C Large U3/U1 Ratio for Average U(i,j) Tensor .... 2.1 PLAT414_ALERT_2_C Short Intra D-H..H-X H7 .. H28A .. 1.98 Ang. PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd. # 1 C17 H16 Br2 N4 S PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -17.133 PLAT905_ALERT_3_C Negative K value in the Analysis of Variance ... -0.679 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 76
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 4 PLAT072_ALERT_2_G SHELXL First Parameter in WGHT Unusually Large. 0.10 PLAT180_ALERT_4_G Check Cell Rounding: # of Values Ending with 0 = 3
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 14 ALERT level C = Check. Ensure it is not caused by an omission or oversight 4 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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