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Acta Cryst. (2013). E69, i32
[ doi:10.1107/S1600536813011033 ]

Tetraammine-2[kappa]4C-[mu]-cyanido-1:2[kappa]2C:N-tricyanido-1[kappa]3C-copper(II)palladium(II)

V. Suchá, J. Kuchár and K. Harms


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Pd1 -- C1 .. 6.5 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Pd1 -- C4 .. 6.5 su PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X) Cu1 -- N5 .. 5.2 su PLAT480_ALERT_4_C Long H...A H-Bond Reported H5B .. N3 .. 2.65 Ang. PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.594 2
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 6 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Pd1 (II) 1.96 PLAT794_ALERT_5_G Note: Tentative Bond Valency for Cu1 (II) 2.11 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 81 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 5 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 4 ALERT type 5 Informative message, check

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