[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o639-o640
[ doi:10.1107/S1600536813008258 ]

(2E)-1-[5-Methyl-1-(4-methylphenyl)-1H-1,2,3-triazol-4-yl]-3-[4-(piperidin-1-yl)phenyl]prop-2-en-1-one

B. F. Abdel-Wahab, E. Abdel-Latif, S. W. Ng and E. R. T. Tiekink


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT910_ALERT_3_B Missing # of FCF Reflections Below Th(Min) ..... 11
Author Response: The lower limit was less than 3 deg., in the standard range for data collections.

Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C45 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C47 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C4 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C28 PLAT334_ALERT_2_C Small Average Benzene C-C Dist. C1 -C6 1.37 Ang. PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0043 Ang PLAT410_ALERT_2_C Short Intra H...H Contact H16 .. H20A .. 1.99 Ang. PLAT410_ALERT_2_C Short Intra H...H Contact H40 .. H44A .. 1.95 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.017
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT093_ALERT_1_G No su's on H-positions, refinement reported as . mixed
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 9 ALERT level C = Check. Ensure it is not caused by an omission or oversight 2 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 7 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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