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[Contents scheme]

Acta Cryst. (2013). E69, m280
[ doi:10.1107/S1600536813010362 ]

Pyridinium bis(pyridine-[kappa]N)tetrakis(thiocyanato-[kappa]N)ferrate(III)-pyrazine-2-carbonitrile-pyridine (1/4/1)

S. I. Shylin, I. A. Gural'skiy, M. Haukka and I. A. Golenya


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT230_ALERT_2_B Hirshfeld Test Diff for S1 -- C1 .. 8.4 su PLAT230_ALERT_2_B Hirshfeld Test Diff for S2 -- C9 .. 9.8 su
Alert level C PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 8
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 1 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00100 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Fe1 -- N3 .. 5.4 su PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C11 - C12 ... 1.45 Ang. PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C18 - C22 ... 1.45 Ang. PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 42
0 ALERT level A = Most likely a serious problem - resolve or explain 2 ALERT level B = A potentially serious problem, consider carefully 1 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 5 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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