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[Contents scheme]

Acta Cryst. (2013). E69, m244-m245
[ doi:10.1107/S1600536813008556 ]

(anti-Chloridothiosemicabazide-[kappa]S)bis(triphenylphosphane-[kappa]P)copper(I) 0.48-hydrate

R. Nimthong, C. Pakawatchai, N. Phongphayak and Y. Wattanakanjana


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms .. ? PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.17 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C25 PLAT420_ALERT_2_C D-H Without Acceptor N3 - H3A ... ? PLAT420_ALERT_2_C D-H Without Acceptor N3 - H3B ... ? PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 5.679
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined D-H Atoms ............ 3 PLAT042_ALERT_1_G Calc. and Reported MoietyFormula Strings Differ ? PLAT128_ALERT_4_G Alternate Setting of Space-group P21/c ....... P21/n PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- Cl1 .. 13.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- S1 .. 12.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- P2 .. 7.7 su PLAT302_ALERT_4_G Note: Anion/Solvent Disorder ................... 100 Perc. PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 4 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 41
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 6 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 7 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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