[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m259-m260
[ doi:10.1107/S160053681300860X ]

Aquabis(4-methylbenzenesulfonato-[kappa]O)([eta]5-pentamethylcyclopentadienyl)rhodium(III) monohydrate

C. P. Roy, P. M. Boyer and J. S. Merola


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B Crystal system given = orthorhombic PLAT355_ALERT_3_B Long O-H Bond (0.82A) O7 - H7B ... 1.12 Ang.
Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O4 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Rh1 PLAT314_ALERT_2_C Check Small Angle for H2O: Metal-O7 -H7A 89.54 Deg. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.594 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 2 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 3 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 49 Perc.
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 7 ALERT level C = Check. Ensure it is not caused by an omission or oversight 3 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 7 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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