[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o750-o751
[ doi:10.1107/S1600536813009276 ]

(1S,3'S,3a'R,6'S)-6'-(2-Chlorophenyl)-3'-[(2R,3S)-1-(4-methoxyphenyl)-4-oxo-3-phenylazetidin-2-yl]-2-oxo-3',3'a,4',6'-tetrahydro-2H,2'H-spiro[acenaphthylene-1,1'-pyrrolo[1,2-c][1,3]thiazole]-2',2'-dicarbonitrile

S. K. Devi, T. Srinivasan, R. Rajesh, R. Raghunathan and D. Velmurugan


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for S1 PLAT915_ALERT_3_C Low Friedel Pair Coverage ...................... 86 Perc.
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K PLAT791_ALERT_4_G Note: The Model has Chirality at C9 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C16 (Verify) S PLAT791_ALERT_4_G Note: The Model has Chirality at C17 (Verify) S PLAT791_ALERT_4_G Note: The Model has Chirality at C18 (Verify) S PLAT791_ALERT_4_G Note: The Model has Chirality at C20 (Verify) R PLAT791_ALERT_4_G Note: The Model has Chirality at C27 (Verify) S PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 39
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 10 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 1 ALERT type 2 Indicator that the structure model may be wrong or deficient 1 ALERT type 3 Indicator that the structure quality may be low 7 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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