Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 5 (May 2013)


organic compounds



xu5691 scheme

Acta Cryst. (2013). E69, o677    [ doi:10.1107/S1600536813008696 ]

N,N'-[2,2'-(Phenylazanediyl)bis(ethane-2,1-diyl)]dipicolinamide

G.-N. Li, Z.-G. Niu, M.-Q. Huang, Y. Zou and L.-J. Hu

Abstract: The asymmetric unit of the title compound, C22H23N5O2, contains two independent molecules with similar conformations; the terminal pyridine rings are oriented at dihedral angles of 23.99 (8) and 18.07 (8)° with respect to the central benzene ring in one molecule and 28.99 (8) and 23.22 (8)° in the other. In the crystal, N-H...O and weak C-H...O hydrogen bonds link the molecules into a three-dimensional supramolecular structure. Weak intermolecular C-H...[pi] interactions are also observed in the crystal.


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