Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 6 (June 2013)

organic compounds

Acta Cryst. (2013). E69, o947-o948    [ doi:10.1107/S1600536813013573 ]

Ethyl 4-anilino-2,6-bis­(4-chloro­phen­yl)-1-phenyl-1,2,5,6-tetra­hydro­pyridine-3-carboxyl­ate

J. Yu, S. Tang, J. Zeng and Z. Yan

Abstract: The title compound, C32H28Cl2N2O2, was synthesized by a multicomponent reaction of 4-chloro­benzaldehyde, aniline and ethyl aceto­acetate. The central 1,2,5,6-tetra­hydro­pyridine ring exhibits a distorted boat conformation and the two chloro­phenyl rings attached to the central ring at positions 2 and 6 are oriented in opposite directions. The two O atoms of the eth­oxy­carbonyl group are involved in intra­molecular N-H...O and C-H...O hydrogen bonds. In the crystal, weak C-H...O hydrogen bonds link mol­ecules related by translation along the b axis into chains.

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