Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 6 (June 2013)

inorganic compounds

Acta Cryst. (2013). E69, i33    [ doi:10.1107/S1600536813011847 ]

(Thio­cyanato-[kappa]S)­tris­(thio­urea-[kappa]S)mercury(II) chloride

A. Shihabuddeen Syed, K. Rajarajan and M. NizamMohideen

Abstract: In the title salt, [Hg(NCS)(CH4N2S)3]Cl, the Hg2+ ion is coordinated in a severely distorted tetra­hedral manner by three thio­urea groups and one thio­cyanate anion through their S atoms. The S-Hg-S angles vary widely from 87.39 (5) to 128.02 (4)°. Weak intra­molecular N-H...S hydrogen bonds are observed, which form S(6) ring motifs. In the crystal, the ions are linked by N-H...N and weak N-H...Cl inter­actions, generating a three-dimensional network.

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