Received 22 March 2013
aDepartment of Physics, Faculty of Arts and Sciences, Ondokuz Mayis University, TR-55139 Samsun, Turkey,bYesilyurt Demir Celik Vocational School, Ondokuz Mayis University, TR-55139 Samsun, Turkey,cDepartment of Chemistry, Amasya Faculty of Arts and Sciences, Ondokuz Mayis University, 05000 Amasya, Turkey,dDepartment of Chemistry, Faculty of Arts and Sciences, Ondokuz Mayis University, Kurupelit, 55139 Samsun, Turkey, and eDepartment of Physics, Faculty of Arts and Sciences, Giresun University, Giresun, Turkey
Correspondence e-mail: email@example.com
The title Schiff base, C23H27ClN2O adopts the phenol-imine tautomeric form, with an intramolecular O-HN hydrogen bond, which generates an S(6) ring motif. Three C atoms of the heterocyclic moiety of the hexahydropyridoquinoline unit, as well as the two methyl groups bonded to one of these C atoms, are disordered over two set of sites, with anoccupancy ratio of 0.740 (4):0.260 (4).
Data collection: CrysAlis PRO (Oxford Diffraction, 2007); cell refinement: CrysAlis PRO; data reduction: CrysAlis PRO; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: ORTEP-3 for Windows (Farrugia, 2012); software used to prepare material for publication: WinGX (Farrugia, 2012).
Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: LR2103 ).
The authors acknowledge the Faculty of Arts and Sciences, Giresun University, Turkey, for the use of the diffractometer
Bernstein, J., Davies, R. E., Shimoni, L. & Chang, N.-L. (1995). Angew. Chem. Int. Ed. Engl. 34, 1555-1573.
Cremer, D. & Pople, J. A. (1975). J. Am. Chem. Soc. 97, 1354-1358.
Farrugia, L. J. (2012). J. Appl. Cryst. 45, 849-854.
Kantar, E. N., Köysal, Y., Gümüs, S., Agar, E. & Soylu, M. S. (2012). Acta Cryst. E68, o1587.
Oxford Diffraction (2007). CrysAlis PRO. Oxford Diffraction Ltd, Abingdon, England.
Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.