[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m311
[ doi:10.1107/S1600536813012403 ]

Tris(N,N-dimethylanilinium) hexabromidostannate(IV) bromide

H. Chouaib, S. Kamoun and H. F. Ayedi


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT234_ALERT_4_C Large Hirshfeld Difference C34 -- C35 .. 0.17 Ang. PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C37 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C38 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Sn1 PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C31 -C36 1.36 Ang. PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C11 -C16 1.37 Ang. PLAT331_ALERT_2_C Small Average Phenyl C-C Dist. C21 -C26 1.36 Ang. PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0085 Ang PLAT414_ALERT_2_C Short Intra D-H..H-X H3B .. H37C .. 1.91 Ang. PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.595 11
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 6 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 4 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for N31B PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for N31A PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 3 % PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF .... # 91 N31B -C38 -N31A 1.555 1.555 1.555 41.20 Deg. PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF .... # 101 N31A -C37 -N31B 1.555 1.555 1.555 39.80 Deg. PLAT779_ALERT_4_G Suspect or Irrelevant (Bond) Angle in CIF .... # 116 N31B -C31 -N31A 1.555 1.555 1.555 39.10 Deg. PLAT794_ALERT_5_G Note: Tentative Bond Valency for Sn1 (IV) 3.51 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 7 PLAT909_ALERT_3_G Percentage of Observed Data at Theta(Max) still 58 %
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 11 ALERT level C = Check. Ensure it is not caused by an omission or oversight 12 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 10 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 4 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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