[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, m335-m336
[ doi:10.1107/S1600536813012981 ]

(Adipato-[kappa]2O,O')diaqua[bis(pyridin-2-yl-[kappa]N)amine]cobalt(II) trihydrate

Z. Setifi, F. Setifi, G. Smith, M. El-Ghozzi, D.-A. Rouag, D. Avignant and H. Merazig


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C6 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 7 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 4
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT154_ALERT_1_G The su's on the Cell Angles are Equal .......... 0.00100 Deg. PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Co1 -- O1 .. 12.3 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Co1 -- O2 .. 21.7 su PLAT790_ALERT_4_G Centre of Gravity not Within Unit Cell: Resd. # 2 H2 O PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 1 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 29
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 8 ALERT level G = General information/check it is not something unexpected 1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 2 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check
checkCIF publication errors
Alert level A PUBL024_ALERT_1_A The number of authors is greater than 5. Please specify the role of each of the co-authors for your paper.
Author Response: Setifi Zouaoui, Rouag Djamil-Azzedine and Merazig Hocine: Synthesis of the title complex. Smith Graham and Setifi Fatima : Preparation of the crystallographic aspects of the article. El-Ghozzi Malika and Avignant Daniel: Data collection and analysis.

1 ALERT level A = Data missing that is essential or data in wrong format 0 ALERT level G = General alerts. Data that may be required is missing

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