Acta Crystallographica Section E

Structure Reports Online

Volume 69, Part 6 (June 2013)

metal-organic compounds

Acta Cryst. (2013). E69, m330    [ doi:10.1107/S160053681301307X ]

Bis(1,4-diazo­niabi­cyclo­[2.2.2]octa­ne) di-[mu]-chlorido-bis­[tetra­chlorido­anti­monate(III)] dihydrate

T. Ben Rhaiem, H. Boughzala and A. Driss

Abstract: The title salt, (C6H14N2)2[Sb2Cl10]·2H2O, was obtained by slow evaporation of an acidic solution of 1,4-di­aza­bicyclo­[2.2.2]octane and SbCl3. The crystal structure consists of (C6H14N2)2+ cations, [Sb2Cl10]4- double octa­hedra and lattice water mol­ecules. All mol­ecular components are situated on special positions. The cation and the lattice water mol­ecule exhibit mirror symmetry, whereas the anion has site symmetry 2/m. The cations, anions and water mol­ecules are alternately arranged into columns along [010]. Individual columns are joined into layers extending along (001). Intra­layer N-H...O and inter­layer N-H...Cl hydrogen-bonding inter­actions lead to the formation of a three-dimensional network.

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