[Open access]

[Contents scheme]

Acta Cryst. (2013). E69, o921-o922
[ doi:10.1107/S1600536813012671 ]

1-Ethyl-2-phenyl-3-[2-(trimethylsilyl)ethynyl]-1H-indole

I. Baglai, V. Maraval, C. Duhayon and R. Chauvin


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level C PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 1 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 PLAT913_ALERT_3_C Missing # of Very Strong Reflections in FCF .... 1
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT128_ALERT_4_G Note: Alternate Setting of Space-group P21/c . P21/n PLAT230_ALERT_2_G Hirshfeld Test Diff for Si20 -- C19 .. 7.1 su PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 13 % PLAT371_ALERT_2_G Long C(sp2)-C(sp1) Bond C3 - C18 ... 1.43 Ang. PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 9 PLAT808_ALERT_5_G No Parseable SHELXL Style Weighting Scheme Found ! PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 6 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 138 PLAT929_ALERT_5_G No Weight Pars,Obs and Calc R1,wR2,S not checked ! PLAT960_ALERT_3_G Number of Intensities with I < - 2*sig(I) ... 5
0 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 3 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 2 ALERT type 2 Indicator that the structure model may be wrong or deficient 6 ALERT type 3 Indicator that the structure quality may be low 3 ALERT type 4 Improvement, methodology, query or suggestion 3 ALERT type 5 Informative message, check

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