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Acta Cryst. (2013). E69, m385-m386  [ doi:10.1107/S1600536813015651 ]

Bis(dicyanamido-[kappa]N)[tris(3-aminopropyl)amine-[kappa]4N]nickel(II)

J. Luo, X.-R. Zhang, L.-J. Qiu, F. Yang and B.-S. Liu


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Alert level B PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 3
Alert level C PLAT213_ALERT_2_C Atom C13' has ADP max/min Ratio ..... 3.2 oblat PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 21
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 7 PLAT003_ALERT_2_G Number of Uiso or Uij Restrained non-H Atoms ... 2 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? Do ! PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N2 .. 5.0 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N5 .. 7.1 su PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Ni1 -- N8 .. 6.3 su PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C13 PLAT242_ALERT_2_G Check Low Ueq as Compared to Neighbors for C13' PLAT301_ALERT_3_G Note: Main Residue Disorder ................... 13 % PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 20 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 5
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 2 ALERT level C = Check. Ensure it is not caused by an omission or oversight 11 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 8 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 1 ALERT type 5 Informative message, check

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