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Acta Cryst. (2013). E69, m373  [ doi:10.1107/S1600536813012841 ]

Pentaaqua(dimethylformamide)cobalt(II) sulfate dimethylformamide monosolvate

M. Tas, S. Çamur and S. Topal


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Alert level B Crystal system given = orthorhombic PLAT922_ALERT_1_B wR2 in the CIF and FCF Differ by ............... -0.0088
Alert level C PLAT230_ALERT_2_C Hirshfeld Test Diff for O4 -- C1 .. 5.7 su PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for Co1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for S1 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N2 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 4.387 PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 3 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 7 PLAT921_ALERT_1_C R1 in the CIF and FCF Differ by ............... -0.0036 PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... -0.101
Alert level G PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite 5 PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF ? PLAT007_ALERT_5_G Note: Number of Unrefined Donor-H Atoms ........ 2 PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints ....... 3 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 25
0 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 10 ALERT level C = Check. Ensure it is not caused by an omission or oversight 5 ALERT level G = General information/check it is not something unexpected 3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 6 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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